(2-溴代烯丙基)三甲硅烷合成路线 （共 17 条）
反应条件
1: 1,2-dibromo-2-propene With trichlorosilane; triethylamine; copper(l) chloride in diethyl ether T=0 - 20°C; 15 h; 2: methylmagnesium bromide in diethyl ether T=0°C; 15 h;
参考文献
Gill, Duncan; Taylor, Nicholas H.; Thomas, Eric J.
Tetrahedron, 2011 , vol. 67, # 27-28 p. 5034 - 5045
反应条件
in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=0°C;
参考文献
Trost, Barry M.; Chan, Dominic M. T.
Journal of the American Chemical Society, 1982 , vol. 104, # 13 p. 3733 - 3735
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; pentane T=0°C; 0.5 h;
参考文献
Trost, Barry M.; Yoshida, Jun-ichi; Lautens, Mark
Journal of the American Chemical Society, 1983 , vol. 105, # 13 p. 4494 - 4496
反应条件
copper(l) iodide in N,N,N',N',N'',N''-hexamethylphosphoric triamide 1.5 h; Ambient temperature;
参考文献
Smith, Janice Gorzynski; Quinn, Nina R.; Viswanathan, Malini
Synthetic Communications, 1983 , vol. 13, # 1 p. 1 - 5
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide 1.5 h; Ambient temperature;
参考文献
Smith, Janice Gorzynski; Drozda, Susan E.; Petraglia, Susan P.; Quinn, Nina R.; Rice, Elizabeth M.; et al.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4112 - 4120
反应条件
in diethyl ether Yield given;
参考文献
Tetrahedron Letters, , vol. 23, # 12 p. 1267 - 1270
Carbohydrate Research, , vol. 171, p. 223 - 232
反应条件
methyl lithium LiBr complex; diethyl ether; copper (I) cyanide 1.) HMPA, THF, 0 deg C, 45 min, 2.) HMPA, THF, 1 h; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 113, # 19 p. 7350 - 7362
反应条件
in diethyl ether 6 h; Ambient temperature;
参考文献
Hollingworth, Gregory J.; Lee, Thomas V.; Sweeney
Synthetic Communications, 1996 , vol. 26, # 6 p. 1117 - 1134
反应条件
lithium perchlorate in diethyl ether
参考文献
Ipaktschi, Junes; Heydari, Akbar
Angewandte Chemie, 1992 , vol. 104, # 3 p. 335 - 336
反应条件
magnesium 1.) THF, reflux, 6 h, 2.) THF, reflux 12 h; Yield given. Multistep reaction;
参考文献
Kang; U
Synthetic Communications, 1994 , vol. 24, # 11 p. 1507 - 1512
