1: 45 percent / lead tetraacetate, pyridine, Cu(OAc)2 / benzene / 3 h / Heating
2: 1) Br2, 2) aq.KOH / 1) CCl4, r.t., 2) 135-145 deg C, 4 h
3: 86.2 percent / conc.H2SO4 / 4 h / Heating
4: 96 percent / LAH / diethyl ether / 2 h / Ambient temperature
5: 90.6 percent / PPTS / CH2Cl2 / 4 h / Ambient temperature
View Scheme
参考文献
Ranganathan, S.; Maniktala, Vibha; Kumar, Raaj; Singh, G. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 12 p. 1197 - 1207
Milburn; Truter
Journal of the Chemical Society, 1954 , p. 3344,3347
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Hougen et al.
Journal of the Chemical Society, 1953 , p. 98,101