反应条件
1: 100 percent / 0.17 h / 600 °C 2: 88.5 percent / diethyl ether / 0.75 h / -78 °C 3: 1.) lithium diisopropylamide / 1.) tetrahydrofuran, hexane, 15 min 2.) 2 h at -78 deg C then 15 h at room temp., HMPA 4: lithium diisopropylamide / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C 5: 90 percent / 30percent H2O2 / CH2Cl2 / 0.08 h / Ambient temperature 6: 83 percent / sodium methoxide / methanol / Ambient temperature View Scheme
参考文献
Salauen, J.; Almirantis, Y.
Tetrahedron, 1983 , vol. 39, # 14 p. 2421 - 2428