2,2,2-三氯乙酰胺苄酯合成路线 （共 52 条）
反应条件
trifluoroacetic acid in dichloromethane; cyclohexane 18 h; Ambient temperature;
参考文献
Iversen, Tommy; Bundle, David R.
Journal of the Chemical Society, Chemical Communications, 1981 , # 23 p. 1240 - 1241
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane 23 h; Ambient temperature;
参考文献
Itoh; Kaneko; Tanami; Yoda
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 9 p. 3356 - 3358
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane
3.5 h; Ambient temperature;
参考文献
Barbier; Schneider; Widmer
Helvetica Chimica Acta, 1987 , vol. 70, # 5 p. 1412 - 1418
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane
T=10 - 20°C; Yield given. Title compound not separated from byproducts;
参考文献
Pons; Kocienski
Tetrahedron Letters, 1989 , vol. 30, # 14 p. 1833 - 1836
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane
Ambient temperature;
参考文献
Seebach, Dieter; Braendli, Urs; Schnurrenberger, Peter; Przybylski, Michael
Helvetica Chimica Acta, 1988 , vol. 71, p. 155 - 167
反应条件
boron trifluoride diethyl etherate in dichloromethane; cyclohexane
24 h; Ambient temperature;
参考文献
Kokotos, George; Chiou, Antonia
Synthesis, 1997 , # 2 p. 168 - 170
反应条件
1: 42.06 g / TfOH / CH2Cl2 / 18 h / 0 °C
2: LiAlH4 / tetrahydrofuran / 6 h / Ambient temperature
View Scheme
参考文献
Halcomb; Huang; Wong
Journal of the American Chemical Society, 1994 , vol. 116, # 25 p. 11315 - 11322
反应条件
1: 72 percent / trifluoromethanesulfonic acid / cyclohexane; CH2Cl2 / 40 h / 20 °C
2: 100 percent / potassium hydroxide / ethanol; H2O / 4 h / 0 °C
View Scheme
参考文献
Kato, Dai-Ichiro; Mitsuda, Satoshi; Ohta, Hiromichi
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7234 - 7242
反应条件
1: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 20 °C / Inert atmosphere
2: methanol; sodium hydroxide / 24 h / 20 °C / Inert atmosphere
3: indium tribromide; 1,1,3,3-tetramethyldisiloxane / toluene / 15 h / 60 °C / Inert atmosphere
View Scheme
参考文献
Pehlivan, Leyla; Metay, Estelle; Delbrayelle, Dominique; Mignani, Gerard; Lemaire, Marc
European Journal of Organic Chemistry, 2012 , # 25 p. 4689 - 4693
反应条件
trifluorormethanesulfonic acid in 1,4-dioxane
T=22°C;
参考文献
Jensen, Thomas; Mikkelsen, Mette; Lauritsen, Anne; Andresen, Thomas L.; Gotfredsen, Charlotte H.; Madsen, Robert
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8886 - 8889
