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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯并蒽酮
合成路线
（共 150 条）
6699-93-0
→
反应条件
82-05-3
苯并蒽酮
反应条件
1: acetic anhydride / Heating 2: 15 percent / K-16 / 550 - 580 °C 3: 69 percent / sodium bichromate / acetic acid / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, # 11 p. 2199 - 2200
Zhurnal Organicheskoi Khimii, , vol. 17, # 11 p. 2462 - 2463
529-34-0
1-四氢萘酮
→
反应条件
82-05-3
苯并蒽酮
反应条件
1: acetic anhydride / Heating 2: 15 percent / K-16 / 550 - 580 °C 3: 69 percent / sodium bichromate / acetic acid / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, # 11 p. 2199 - 2200
Zhurnal Organicheskoi Khimii, , vol. 17, # 11 p. 2462 - 2463
138642-62-3
2-氰基苯硼酸
→
反应条件
82-05-3
苯并蒽酮
+
6051-98-5
7h-苯并(c)芴-7-酮
反应条件
1: toluene / 2 h / 110 °C 2: Pd(PPh3)2Cl2; K3PO4 / toluene / 12 h / 100 °C / |Schlenk technique; |Inert atmosphere 3: water; silver trifluoroacetate; dichloro bis(acetonitrile) palladium(II) / trifluoroacetic acid; N,N-dimethyl acetamide / 68 h / 140 °C / |Glovebox; |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 11 p. 2742 - 2745
81-96-9
3-溴苯并蒽酮
→
反应条件
82-05-3
苯并蒽酮
+
116-71-2
反应条件
1: With [2,2']bipyridinyl; nickel dichloride; zinc in N,N-dimethyl-formamide T=60°C; 6 h; 2: With dihydrogen peroxide in N,N-dimethyl-formamide T=30 - 40°C; 0.5 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 36, # 6 p. 861 - 865
13922-41-3
+
6630-33-7
→
反应条件
82-05-3
苯并蒽酮
+
6051-98-5
7h-苯并(c)芴-7-酮
反应条件
1.1: sodium carbonate / N,N-dimethyl-formamide; water / 0.08 h 1.2: 20 °C 2.1: tert.-butylhydroperoxide; biscyclopentadienyliron(II) / acetonitrile; decane / 24 h / 20 - 90 °C View Scheme
参考文献
Organic Letters, , vol. 15, # 4 p. 928 - 931
90-14-2
+
172732-52-4
→
反应条件
82-05-3
苯并蒽酮
+
6051-98-5
7h-苯并(c)芴-7-酮
反应条件
1: Pd(PPh3)2Cl2; K3PO4 / toluene / 12 h / 100 °C / |Schlenk technique; |Inert atmosphere 2: water; silver trifluoroacetate; dichloro bis(acetonitrile) palladium(II) / trifluoroacetic acid; N,N-dimethyl acetamide / 68 h / 140 °C / |Glovebox; |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 11 p. 2742 - 2745
66252-14-0
→
反应条件
82-05-3
苯并蒽酮
反应条件
1: IPy2BF4; tetrafluoroboric acid / dichloromethane; diethyl ether / 24 h / -70 °C 2: palladium diacetate; triphenylphosphine; triethylamine / water; N,N-dimethyl-formamide / 22 h / 130 °C / |Inert atmosphere View Scheme
参考文献
European Journal of Organic Chemistry, , # 29 p. 6491 - 6495
13922-41-3
→
反应条件
82-05-3
苯并蒽酮
反应条件
1: palladium diacetate; potassium carbonate / water; N,N-dimethyl-formamide / 2 h / 20 °C 2: IPy2BF4; tetrafluoroboric acid / dichloromethane; diethyl ether / 24 h / -70 °C 3: palladium diacetate; triphenylphosphine; triethylamine / water; N,N-dimethyl-formamide / 22 h / 130 °C / |Inert atmosphere View Scheme
参考文献
European Journal of Organic Chemistry, , # 29 p. 6491 - 6495
2042-37-7
→
反应条件
82-05-3
苯并蒽酮
反应条件
1: palladium diacetate; potassium carbonate / water; N,N-dimethyl-formamide / 2 h / 20 °C 2: IPy2BF4; tetrafluoroboric acid / dichloromethane; diethyl ether / 24 h / -70 °C 3: palladium diacetate; triphenylphosphine; triethylamine / water; N,N-dimethyl-formamide / 22 h / 130 °C / |Inert atmosphere View Scheme
参考文献
European Journal of Organic Chemistry, , # 29 p. 6491 - 6495
90-44-8
→
反应条件
82-05-3
苯并蒽酮
反应条件
sulfuric acid T=70°C;
参考文献
US2295649 , ;
DE699771 , ;
DRP/DRBP Org.Chem.
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