2-甲基-2-丙烯基乙酸酯合成路线 （共 57 条）
反应条件
9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; sodium acetate 1.) THF, 25 deg C, 1 h, 2.) room temp.; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 46, # 20 p. 3978 - 3988
反应条件
1: Methallyl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 2: monoiodonaphthalene in N,N-dimethyl-formamide T=100°C;
参考文献
Seomoon, Dong; Lee, Kooyeon; Kim, Hyunseok; Lee, Phil Ho
Chemistry - A European Journal, 2007 , vol. 13, # 18 p. 5197 - 5206
反应条件
aluminum oxide; potassium fluoride; potassium fluoride on basic alumina; 1,2-bis-(diphenylphosphino)ethane; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran 144 h; Ambient temperature;
参考文献
Muzart, J.; Genet, J.-P.; Denis, A.
Journal of Organometallic Chemistry, 1987 , vol. 326, p. C23 - C28
反应条件
1: With oxygen; trifluoroacetic acid in acetonitrile T=60°C; P=760.051 Torr; 2: With triphenylphosphine in acetonitrile T=20°C;
参考文献
Jasch, Hannelore; Hoefling, Sarah B.; Heinrich, Markus R.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1520 - 1532
反应条件
bis(acetylacetonato) palladium in 1,4-dioxane T=145 - 160°C; 15 h;
参考文献
Malet; Moreno-Manas; Pleixats
Synthetic Communications, 1992 , vol. 22, # 15 p. 2219 - 2228
反应条件
1: Methallyl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 2: monoiodonaphthalene in N,N-dimethyl-formamide T=100°C;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1641 - 1645
反应条件
1: Methallyl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 2: 3-methoxy-iodobenzene in N,N-dimethyl-formamide T=100°C;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1641 - 1645
反应条件
1: Methallyl acetate With manganese; trifluoroacetic acid; cobalt(II) dibromide in acetonitrile T=20°C; 0.0833333 h; 2: ethyl 4-bromobutanoate With pyridine in acetonitrile T=80°C;
参考文献
Qian, Xin; Auffrant, Audrey; Felouat, Abdellah; Gosmini, Corinne
Angewandte Chemie - International Edition, 2011 , vol. 50, # 44 p. 10402 - 10405
反应条件
hydrogen; C52H42N2O6P2; dicarbonyl(2,2,6,6-tetramethyl-3,5-heptanedionato)rhodium in toluene T=90°C; P=3878.71 - 7757.43 Torr; 4 h;
参考文献
E. I. du Pont de Nemours and Company
Patent: US6664427 B1, 2003 ;
Location in patent: Page column 19 ;
反应条件
1.1: AlCl3, aluminium chloride; Propylene glycol / methyl acetate / 0 - 5 °C 2.1: AlCl3, aluminium chloride / dichloromethane / 2.33 h / -5 - 0 °C 2.2: 5 h / 0 °C View Scheme
参考文献
Ronggeng, Wang; Yougui, Zhao; Guanchao, Zhang
Research on Chemical Intermediates, 2013 , vol. 39, # 5 p. 2149 - 2155
