2-甲基-2-丙烯基乙酸酯合成路线 （共 57 条）
反应条件
tris-(dibenzylideneacetone)dipalladium(0) in dimethyl sulfoxide T=60°C; Miyaura reaction; 12 h; Inert atmosphere;
参考文献
Zhang, Ping; Brozek, Laura A.; Morken, James P.
Journal of the American Chemical Society, 2010 , vol. 132, # 31 p. 10686 - 10688
反应条件
dilithium tetrachlorocuprate in tetrahydrofuran; diethyl ether
参考文献
Schlosser,M. et al.
Helvetica Chimica Acta, 1974 , vol. 57, p. 1567 - 1576
反应条件
copper acetylacetonate in tetrahydrofuran T=-8°C; 0.5 h;
参考文献
Julia, Marc; Righini-Tapie, Anne; Verpeaux, Jean-Noel
Tetrahedron, 1983 , vol. 39, # 20 p. 3283 - 3288
反应条件
Pd[P(OPh)3]4 T=160°C; 3 h; var. catalysts, var. temp., var. time, high pressure; Product distribution;
参考文献
Urata, Hisao; Suzuki, Hiroharu; Moro-oka, Yoshihiko; Ikawa, Tsuneo
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 2 p. 607 - 608
反应条件
Pd[P(OPh)3]4 T=160°C; 3 h; var. catalysts, var. temp., var. time, high pressure; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 2 p. 607 - 608
参考文献
N.V.de Bataafsche Petr.Mij.
Patent: FR789033 , 1935 ;
Full Text Show Details
Shell Devel.Co.
Patent: US2046556 , 1934 ;
反应条件
in dichloromethane
Refluxing of Fe-complex (prepd. in situ) and methylallyacetate with stirring for 2 h.; Cooling, chromy. (silica gel, hexane-ethylacetate) gives iron complex and p-tolyl vinyl ketone.;
参考文献
Itoh, Keiji; Nakanishi, Saburo; Otsuji, Yoshio
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 10 p. 2965 - 2977
反应条件
Ni(1,4-bis(diphenylphosphanyl)butane)2; nBu4NPF6 in N,N-dimethyl-formamide
T=50°C; time dependence; Product distribution;
参考文献
Bricout, Herve; Carpentier, Jean-Francois; Mortreux, Andre
Tetrahedron, 1998 , vol. 54, # 7 p. 1073 - 1084
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
0.5 h; Ambient temperature;
参考文献
Tsuda, Tetsuo; Okada, Masahiro; Nishi, Sei-ichi; Saegusa, Takeo
Journal of Organic Chemistry, 1986 , vol. 51, # 4 p. 421 - 426
反应条件
AlCl3, aluminium chloride; Propylene glycol in methyl acetate
T=0 - 5°C;
参考文献
Ronggeng, Wang; Yougui, Zhao; Guanchao, Zhang
Research on Chemical Intermediates, 2013 , vol. 39, # 5 p. 2149 - 2155
