1,4-二氯-2-丁炔合成路线 （共 101 条）
反应条件
potassium carbonate in acetone Heating; Yield given. Yields of byproduct given;
参考文献
Conti, Paola; Dallanoce, Clelia; De Amici, Marco; De Micheli, Carlo; Ebert, Bjarke
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 8 p. 1033 - 1036
参考文献
Schostakovskii,M.F.; Khomenko,A.Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1960 , p. 1022 - 1026
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , p. 1098 - 1103
反应条件
in hexane Ar, to a filtered soln. of Ti compd. added a soln. of alkyne with stirring, allowed to stand at 20°C for 24 h; filtered, concd. (vac.), cooled to -78°C for 1 d, decanted, crysts. washed (cold hexane), dried (vac.); elem. anal.;
参考文献
Burlakov, Vladimir V.; Arndt, Perdita; Baumann, Wolfgang; Spannenberg, Anke; Rosenthal, Uwe; Parameswaran, Pattiyil; Jemmis, Eluvathingal D.
Chemical Communications, 2004 , # 18 p. 2074 - 2075
反应条件
in benzene byproducts: CCCH2CH2P(C4H9)3, P(CH3)3; (N2);
参考文献
Breen, Tricia L.; Stephan, Douglas W.
Journal of the American Chemical Society, 1995 , vol. 117, # 48 p. 11914 - 11921
参考文献
Chomenko; Gorban
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 1676;engl.Ausg.S.1611
反应条件
tellurium; sodium tetrahydroborate; potassium hydroxide in 1,4-dioxane; water Inert atmosphereCooling with ice;
参考文献
Jahnke, Ashlee A.; Howe, Graeme W.; Seferos, Dwight S.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 52 p. 10140 - 10144
参考文献
Iwai,I.; Tomita,K.
Chemical and Pharmaceutical Bulletin, 1961 , vol. 9, p. 976 - 979
参考文献
Gillespie, Donal G.; Walker, Brian J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1689 - 1695
参考文献
Chang, Sukbok; Lee, Nam Ho; Jacobsen, Eric N.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 6939 - 6941
反应条件
magnesium in diethyl ether 3 h; Heatingother dihaloaryls, other dihalobutenes; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 46, # 10 p. 2194 - 2196
