双环庚烯(3.2.1)-2-辛烯合成路线 (共 14 条)
反应条件
ammonia; sodium in pentane T=-78°C;
参考文献
Clark, J. Stephen; Clarke, Melanie-Rose; Clough, John; Blake, Alexander J.; Wilson, Claire
Tetrahedron Letters, 2004 , vol. 45, # 51 p. 9447 - 9450
反应条件
sodium in various solvent(s) T=80 - 110°C; 1 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 54, # 22 p. 5286 - 5292
反应条件
sodium; tert-butyl alcohol in tetrahydrofuran 40 h; Heating;
参考文献
Eggimann, Thomas; Ibrahim, Nan; Shaw, R. Anthony; Wieser, Hal
Canadian Journal of Chemistry, 1993 , vol. 71, # 4 p. 578 - 610
反应条件
1: 52 percent / aq. NaOH; PhCH2NEt3(1+)*Cl(1-); CHCl3 / 20 °C 2: 80 percent / lithium aluminum hydride / tetrahydrofuran / 20 °C 3: 52 percent / sodium; ammonia (liq.) / pentane / -78 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 51 p. 9447 - 9450
参考文献
Chemische Berichte, , vol. 103, p. 1637 - 1644
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 248, p. 3301
Bulletin de la Societe Chimique de France, , p. 473,478
参考文献
Chemische Berichte, , vol. 88, p. 144,153
Chemische Berichte, , vol. 91, p. 1516,1524
Suomen Kemistilehti B, , vol. 38, p. 260,263,267,272
反应条件
sodium acetate; sodium nitrite Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 8 p. 1369 - 1376
反应条件
sodium acetate; sodium nitrite Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 8 p. 1369 - 1376
反应条件
solvolysis in 80percent aq. THF, 40 deg C, 10 d; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 8 p. 1369 - 1376