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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
82437-75-0
合成路线
（共 37 条）
66107-29-7
4-甲氧基三氟甲烷磺酸苯酯
→
反应条件
82437-75-0
反应条件
caesium carbonate; tri-cyclo-hexyl-phosphine; palladium diacetate in tetrahydrofuran Suzuki-Miyaura reaction; 48 h; Heating;
参考文献
Molander, Gary A.; Petrillo, Daniel E.; Landzberg, Nicole R.; Rohanna, John C.; Biolatto, Betina
Synlett, 2005 , # 11 art. no. Y00205ST, p. 1763 - 1766
10486-61-0
3-碘噻吩
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
82437-75-0
反应条件
potassium carbonate in water; acetone T=60°C; Suzuki coupling; 5 h;
参考文献
Mejias, Nereida; Pleixats, Roser; Shafir, Alexandr; Medio-Simon, Mercedes; Asensio, Gregorio
European Journal of Organic Chemistry, 2010 , # 26 p. 5090 - 5099
17249-80-8
3-氯噻吩
+
623-12-1
→
反应条件
82437-75-0
反应条件
1: 1-methoxy-4-chlorobenzene With tetrahydroxydiboron; ethanol; (X-phos)palladium(II) phenethylamine chloride; potassium acetate; sodium t-butanolate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=80°C; 2 h; Inert atmosphere; 2: thien-3-yl chloride With potassium carbonate in ethanol; water T=80°C; Suzuki-Miyaura reaction; 15 h; Inert atmosphere;
参考文献
Molander, Gary A.; Trice, Sarah L. J.; Dreher, Spencer D.
Journal of the American Chemical Society, 2010 , vol. 132, # 50 p. 17701 - 17703
104-92-7
→
反应条件
82437-75-0
反应条件
palladium diacetate; tris-(o-tolyl)phosphine in toluene T=20°C; 5 h; Inert atmosphere; SolventReagent/catalystConcentration;
参考文献
Chen, Xu; Zhou, Lingmin; Li, Yimei; Xie, Tao; Zhou, Shuangliu
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 230 - 239
82437-74-9
→
反应条件
82437-75-0
反应条件
copper in quinoline 1 h; Heating;
参考文献
Kirsch; Prim
Synthetic Communications, 1994 , vol. 24, # 12 p. 1721 - 1726
872-31-1
+
13139-86-1
→
反应条件
82437-75-0
+
2132-80-1
反应条件
triphenylphosphine; Pd bipyridyl anchored nanosized mesoporous silica MCM-41 in tetrahydrofuran Kumada-Corriu reaction; 24 h; Heating;
参考文献
Tsai, Fu-Yu; Lin, Bo-Nan; Chen, Ming-Jie; Mou, Chung-Yuan; Liu, Shiuh-Tzung
Tetrahedron, 2007 , vol. 63, # 20 p. 4304 - 4309
188290-36-0
+
696-62-8
→
反应条件
82437-75-0
+
42545-43-7
反应条件
potassium tert-butylate in dimethyl sulfoxide T=20°C; 3 h; Schlenk techniqueInert atmosphereIrradiation; TimeTemperatureConcentrationReagent/catalyst; Overall yield = 90 percent;
参考文献
Buden, Maria E.; Guastavino, Javier F.; Rossi, Roberto A.
Organic Letters, 2013 , vol. 15, # 6 p. 1174 - 1177
100-66-3
→
反应条件
82437-75-0
反应条件
1: 34 percent / AlCl3 / CH2Cl2 / 5 deg C., 30 min., than RT, 1 h 2: 86 percent / H2, KOH / 10percent Pd(C) / methanol / 1 h / Ambient temperature View Scheme
参考文献
Sone, Tyo; Inoue, Manabu; Sato, Kazuaki
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 10 p. 3779 - 3781
188290-36-0
+
98-68-0
→
反应条件
82437-75-0
反应条件
dichloro bis(acetonitrile) palladium(II); lithium carbonate in 1,4-dioxane T=140°C; 40 h; Schlenk technique; regioselective reaction;
参考文献
Yuan, Kedong; Doucet, Henri
Chemical Science, 2013 , vol. 5, # 1 p. 392 - 396
872-31-1
+
104-92-7
→
反应条件
82437-75-0
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II); magnesium 1.) Et2O, 2.) heating, 24 h;
参考文献
Montheard, Jean-Pierre; Delzant, Jean-Francois; Gazard, Maryse
Synthetic Communications, 1984 , vol. 14, # 3 p. 289 - 292
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