1,5-二甲基-6-氧杂双环[3.1.0]己烷合成路线 (共 7 条)
反应条件
polystyrene-supported methyltrioxorhenium; dihydrogen peroxide in tert-butyl alcohol
T=40°C; 72 h; Further byproducts given;
参考文献
Bianchini, Gianluca; Crucianelli, Marcello; Canevali, Carmen; Crestini, Claudia; Morazzoni, Franca; Saladino, Raffaele
Tetrahedron, 2006 , vol. 62, # 52 p. 12326 - 12333
反应条件
3-chloro-benzenecarboperoxoic acid in tetrachloromethane
T=0°C; Rate constant;
参考文献
Friedrich,L.E.; Fiato,R.A.
Journal of the American Chemical Society, 1974 , vol. 96, # 18 p. 5783 - 5787
反应条件
in dichloromethane
T=-20°C; 8 h;
参考文献
Adam, Waldemar; Andler, Simone; Heil, Markus
Angewandte Chemie, 1991 , vol. 103, # 10 p. 1395 - 1396
参考文献
Bartlett; Bavley
Journal of the American Chemical Society, 1938 , vol. 60, p. 2416,2417
反应条件
oxygen; ozone in gas
0.166667 h; Ambient temperature; Further byproducts given;
参考文献
Griesbaum, Karl; Miclaus, Vasile; Jung, Chan; Quinkert, Ralf-Olaf
European Journal of Organic Chemistry, 1998 , # 4 p. 627 - 629
反应条件
oxygen; ozone in gas
0.166667 h; Ambient temperature; Product distribution;
参考文献
Griesbaum, Karl; Miclaus, Vasile; Jung, Chan; Quinkert, Ralf-Olaf
European Journal of Organic Chemistry, 1998 , # 4 p. 627 - 629
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile
1 h; Ambient temperature;
参考文献
Roy, Subhas Chandra; Adhikari, Sankar
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 7 p. 459