2-重氮乙酰乙酸对硝基苄酯合成路线 (共 5 条)
反应条件
triethylamine in toluene
参考文献
Merck and Co., Inc.
Patent: US5340927 A1, 1994 ;
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane T=23°C;
参考文献
Meyer, Michael E.; Ferreira, Eric M.; Stoltz, Brian M.
Chemical Communications, 2006 , # 12 p. 1316 - 1318
反应条件
triethylamine in acetonitrile
反应条件
4-toluenesulfonyl azide; triethylamine in acetonitrile 3 h; Ambient temperature;
参考文献
Ueda; Roberge; Vinet
Canadian Journal of Chemistry, 1984 , vol. 62, # 12 p. 2936 - 2940
反应条件
1: 76.6 percent / toluene / 15 h / Heating 2: 90.4 percent / triethylamine, p-toluenesulfonyl azide / acetonitrile / 3 h / Ambient temperature View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 62, # 12 p. 2936 - 2940