1: With 2-hydroxy-1,3-isoindolinedione; 2,2'-azo-bisisobutyronitrile; oxygen in acetonitrile T=75°C; P=760 Torr; 3 h; 2: With sulfuric acid in acetonitrile T=25°C; 2 h; Further byproducts given;
EXXONMOBIL CHEMICAL PATENTS INC.; PATEL, Bryan, A.; BENITEZ, Francisco, M.; SMITH, Charles, M.; DAKKA, Jihad, M.; REINE, Travis, A.
Patent: WO2013/95791 A1, 2013 ;
Location in patent: Paragraph 0095 ;
oxygen; 2,2'-azo-bisisobutyronitrile T=120°C; 12 h; various temperatures: 130 deg. C, 140 deg. C various conc. of catalyst; Product distributionThermodynamic dataMechanism;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, # 4 p. 654 - 659
Zhurnal Organicheskoi Khimii, , vol. 16, # 4 p. 745 - 751
oxygen; 2,2'-azo-bisisobutyronitrile T=120°C; 12 h; various temperatures: 130 deg. C, 140 deg. C various conc. of catalyst; Product distributionThermodynamic dataMechanism;
参考文献
Velyutin, L. P.; Potekhin, V. M.; Ovchinnikov, V. I.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 4 p. 654 - 659
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 4 p. 745 - 751
