2,4-二甲氧基苯乙酮合成路线 （共 100 条）
反应条件
1: AlCl3; benzene / 100 - 110 °C 2: acetic acid; nitric acid View Scheme
参考文献
Shinoda; Sato; Kawagoye
Yakugaku Zasshi, 1932 , vol. 52, p. 766,773;dtsch.Ref.S.91
Chem.Abstr., 1933 , p. 295
反应条件
copper(ll) bromide in chloroform; ethyl acetate 10 h; Inert atmosphereReflux;
参考文献
Al-Rifai, Nafisah; Ruecker, Hannelore; Amslinger, Sabine
Chemistry - A European Journal, 2013 , vol. 19, # 45 p. 15384 - 15395
反应条件
(i) PhCO3H, TsOH, (ii) aq. KOH; Multistep reaction;
参考文献
Bulletin de la Societe Chimique de France, , p. 1003 - 1007
反应条件
toluene-4-sulfonic acid; acetic acid T=35°C; zuletzt bei 60-65grad, und Erwaermen des Reaktionsprodukts mit wss.-aethanol. H2SO4;
参考文献
Gazzetta Chimica Italiana, , vol. 79, p. 924,927
反应条件
und Erwaermen des Reaktionsprodukts mit wss.-aethanol.H2SO4;
参考文献
Gazzetta Chimica Italiana, , vol. 79, p. 924,927
反应条件
sodium hydroxide in methanol T=28°C; Claisen Schmidt condensation;
参考文献
Liu; Wilairat; Go
Journal of Medicinal Chemistry, 2001 , vol. 44, # 25 p. 4443 - 4452
反应条件
ethylene glycol; perchloric acid in benzene 2 h; Heatingother equiv of catalyst, other time; TsOH;
参考文献
Journal of Organic Chemistry, , vol. 49, # 15 p. 2663 - 2669
反应条件
toluene-4-sulfonic acid in benzene 2 h; Heatingother equiv of catalyst, other time; HClO4; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 49, # 15 p. 2663 - 2669
反应条件
1: diethyl ether; sodium amide 2: hydriodic acid View Scheme
参考文献
Journal of the Chemical Society, , vol. 113, p. 876
反应条件
1: sodium 2: concentrated hydriodic acid View Scheme
参考文献
v. Kostanecki; Rozycki
Chemische Berichte, 1901 , vol. 34, p. 3726
