2,5-二甲基-1-苯基吡咯合成路线 (共 24 条)
参考文献
Organic Letters, , vol. 6, # 17 p. 2957 - 2960
反应条件
9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene 24 h; Heating; Title compound not separated from byproducts.;
参考文献
Tetrahedron Letters, , vol. 48, # 29 p. 5115 - 5120
反应条件
diethyl ether; benzene
参考文献
Collection of Czechoslovak Chemical Communications, vol. 1, p. 286
Chem. Zentralbl., , vol. 100, # II p. 719
反应条件
Leiten ueber Palladium/Asbest bei 400grad;
参考文献
Doklady Akademii Nauk SSSR, , vol. 88, p. 845,847
Chem.Abstr., , p. 3338
参考文献
Chemische Berichte, , vol. 18, p. 306,307
Justus Liebigs Annalen der Chemie, , vol. 236, p. 303
参考文献
Collect.Trav.chim.Tschecosl., vol. 1, p. 283,285,286
Chem. Zentralbl., , vol. 100, # II p. 719
反应条件
acetic acid in water T=50°C; 3 h;
参考文献
Porretta; Biava; Fioravanti; Villa; Simonetti
Farmaco, 1991 , vol. 46, # 7-8 p. 987 - 995
反应条件
sodium tetrahydroborate; oxygen; ozone 1. -78 degC, dichloromethane; 2. ethanol, r.t., overnight; Yield given. Multistep reaction;
参考文献
Kashima, Choji; Hibi, Shigeki; Maruyama, Tatsuya; Harada, Kazuo; Omote, Yoshimori
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 637 - 639
反应条件
trichlorophosphate
T=110°C; 6 h;
参考文献
Mao, Yongjun; Lin, Nan; Tian, Wang; Huang, Ziwei; An, Jing
Heterocycles, 2012 , vol. 85, # 5 p. 1179 - 1185
反应条件
1: With N,N-dimethyl-formamide; trichlorophosphate in toluene
T=80°C; 3 h;
2: With water; sodium carbonate in toluene
T=20°C; Product distribution / selectivity;
参考文献
REGENTS OF THE UNIVERSITY OF CALIFORNIA
Patent: US2008/293766 A1, 2008 ;
Location in patent: Page/Page column 10 ;