2,4,6-三羟基苯甲酸合成路线 (共 56 条)
反应条件
sodium periodate in methanol T=25°C; KineticsRate constant;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 4 p. 737 - 744
反应条件
β-CD; potassium chloride; potassium hydroxide ElectrolysisInert atmosphere;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 76, # 12 p. 1651 - 1667
参考文献
Monatshefte fuer Chemie, , vol. 22, p. 219
反应条件
formic acid; water in methanol pH=1.7; Pulsed electric field; Kinetics;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 58, # 6 p. 3524 - 3531
参考文献
Zeitschrift fuer Physikalische Chemie, Stoechiometrie und Verwandtschaftslehre, , vol. 93, p. 183
参考文献
Monatshefte fuer Chemie, , vol. 22, p. 219
参考文献
Justus Liebigs Annalen der Chemie, , vol. 351, p. 319
参考文献
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, , vol. <5> 10 II, p. 241
反应条件
1: 34 percent / trifluoroacetic anhydride / trifluoroacetic acid / 24 h / Ambient temperature 2: 92 percent / triphenylphosphine, DIAD / tetrahydrofuran / 2 h / 0 - 20 °C 3: 85 percent / pyridine / 12 h / 0 °C 4: 87 percent / bis(triphenylphosphine)palladium(II) chloride, Et3N / dimethylformamide / 12 h / 90 °C 5: 100 percent / H2 / Pd(OH)2 / ethanol / 12 h / 760 Torr 6: 99 percent / 48percent aq. KOH / dimethylsulfoxide / 4.5 h / 115 °C View Scheme
参考文献
Dushin; Danishefsky
Journal of the American Chemical Society, 1992 , vol. 114, # 2 p. 655 - 659
反应条件
1.1: 93 percent / K2CO3 / acetone / 24 h / 20 °C 2.1: DIPEA / CH2Cl2 / 4 h 2.2: 77 percent / NaH / dimethylformamide / 0.5 h 3.1: 96 percent / LiAlH4 / diethyl ether / 0 - 20 °C 4.1: 88 percent / tetrapropylammonium perruthenate; N-methylmorpholine-N-oxide / CH2Cl2 / 1 h View Scheme
参考文献
Henry, Kevin M.; Townsend, Craig A.
Journal of the American Chemical Society, 2005 , vol. 127, # 10 p. 3300 - 3309