2-羟基-1,4-萘醌合成路线 (共 313 条)
反应条件
5,6-O-isopropylidene-L-ascorbic acid in ethylene glycol dimethyl ether 20 h; UV-irradiation;
参考文献
Kulkarni, Mukund G.; Kate, Sandesh D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 24 p. 4242 - 4244
参考文献
Graebe; Ludwig
Justus Liebigs Annalen der Chemie, 1870 , vol. 154, p. 307
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Tommasi
Gazzetta Chimica Italiana, 1920 , vol. 50 I, p. 268
参考文献
Tommasi
Gazzetta Chimica Italiana, 1920 , vol. 50 I, p. 268
反应条件
ammonium cerium (IV) nitrate in acetonitrile T=0 - 20°C; 4 h; Overall yield = 61 percent;
参考文献
Sivan, Akhil; Deepthi, Ani
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1890 - 1893
反应条件
hydrogenchloride; sodium hydroxide; sodium nitrite T=0°C; 1 h;
参考文献
Gleiter, Rolf; Dobler, Walter
Chemische Berichte, 1985 , vol. 118, # 12 p. 4725 - 4742
反应条件
1: 40 percent / lithium hydride / dimethylsulfoxide / 45 deg C, 5 h; 25 deg C, 10 h 2: m-chloroperoxybenzoic acid / CH2Cl2 / 17 h / 25 °C 3: 67 percent / BF3*OEt2 / CH2Cl2 / 21 h / 25 °C View Scheme
参考文献
Sun, Jerry S.; Geiser, Andrew H.; Frydman, Benjamin
Tetrahedron Letters, 1998 , vol. 39, # 45 p. 8221 - 8224
反应条件
N-methylamine hydrochloride; toluene-4-sulfonic acid in toluene 5 h; RefluxDean-Stark;
参考文献
Da Rocha, David R.; Mota, Kelly; Da Silva, Illana M.C.B.; Ferreira, Vitor F.; Ferreira, Sabrina B.; Da Silva, Fernando De C.
Tetrahedron, 2014 , vol. 70, # 20 p. 3266 - 3270
反应条件
thionyl chloride Heating;
参考文献
Synlett, , # 16 p. 2569 - 2573
反应条件
1: 36 percent / triethylamine / acetonitrile / 1.33 h / Heating 2: 23 percent / triethylamine / toluene / 7 h / Heating View Scheme
参考文献
Bock, Klaus; Jacobsen, Niels; Terem, Bulent
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 659 - 664
反应条件
1: Ac2O 2: Zn, NaOAc 3: aq. H2SO4 / ethanol View Scheme
参考文献
Beaumont,P.C.; Edwards,R.L.
Journal of the Chemical Society [Section] C: Organic, 1971 , vol. <C>, p. 1000 - 1004