2-羟基-1,4-萘醌合成路线 (共 313 条)
反应条件
toluene-4-sulfonic acid in chloroform T=20°C; 24 h;
参考文献
Koulouri, Sofia; Malamidou-Xenikaki, Elizabeth; Spyroudis, Spyros
Tetrahedron, 2005 , vol. 61, # 46 p. 10894 - 10902
反应条件
1: 92 percent / concd. H2SO4 / benzene / 1.5 h / Heating
2: 4 percent / acetonitrile / 0.5 h / Irradiation
3: 7.5 mg / H2 / 10percent Pd-C / methanol / 1 h / Ambient temperature
View Scheme
参考文献
Moser; Paulshock
Journal of the American Chemical Society, 1950 , vol. 72, p. 5419,5423
反应条件
Oxonereg;; NH4Br in methanol
0.25 h; Reflux; regioselective reaction;
参考文献
MacHarla, Arun Kumar; Chozhiyath Nappunni, Rohitha; Marri, Mahender Reddy; Peraka, Swamy; Nama, Narender
Tetrahedron Letters, 2012 , vol. 53, # 2 p. 191 - 195
参考文献
Diehl; Merz
Chemische Berichte, 1878 , vol. 11, p. 1065
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in acetonitrile
T=20°C;
参考文献
Patil, Pravin; Nimonkar, Abhay; Akamanchi, Krishnacharya G.
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2331 - 2336
反应条件
in acetonitrile
1.5 h; Irradiation;
参考文献
Thaplial, Prakash Chander
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1998 , vol. 37, # 5 p. 477 - 479
反应条件
hydrogenchloride; potassium hydroxide
T=45°C;
参考文献
Neunhoeffer; Weise
Chemische Berichte, 1938 , vol. 71, p. 2703,2707
反应条件
1: K2CO3 / acetone / 40 h / Heating
2: 70 mg / zinc dust / tetrahydrofuran / 24 h
View Scheme
参考文献
Kapoor, N. K.; Gupta, R. B.; Khanna, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 189 - 191
参考文献
Tommasi
Gazzetta Chimica Italiana, 1920 , vol. 50 I, p. 268
反应条件
1: 65 percent / 2,6-lutidine, DMAP / CH2Cl2 / 3 h / 23 °C
2: 73 percent / NMP / Pd2(dba)3*dba / 16 h / 23 °C
View Scheme
参考文献
Best, Wayne M.; Sims, Colette G.; Winslade, Merilyn
Australian Journal of Chemistry, 2001 , vol. 54, # 6 p. 401 - 404