2-羟基-1,4-萘醌合成路线 (共 313 条)
反应条件
Reaktion des essigsaures Salzes;
参考文献
Elsbach
Chemische Berichte, 1882 , vol. 15, p. 689
反应条件
diethyl ether; acetic acid
T=90°C;
参考文献
Fieser et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 3177
反应条件
5,10,15,20-tetrakis-pentafluorophenyl-21H,23H-porphyrin iron(III) chloride; dihydrogen peroxide in methanol; dichloromethane
Oxidation;
参考文献
Cunningham, Ian D.; Danks, Timothy N.; O'Connell, Keith T. A.; Scott, Peter W.
Journal of Organic Chemistry, 1999 , vol. 64, # 20 p. 7330 - 7337
反应条件
potassium hydroxide; sodium dithionite; tetrabutylammomium bromide
1.) H2O, THF, room temperature, 15 min, 2.) 10 h; Yield given. Multistep reaction;
参考文献
Kraus, George; Man, Tim On
Synthetic Communications, 1986 , vol. 16, # 9 p. 1037 - 1042
反应条件
sodium hydroxide; hydroxylamine hydrochloride
参考文献
v.Kostanecki
Chemische Berichte, 1889 , vol. 22, p. 1343
反应条件
ammonium cerium(IV) nitrate in acetonitrile
T=0°C;
参考文献
Kobayashi, Kazuhiro; Uneda, Tomokazu; Tanaka, Koujirou; Mori, Masako; Tanaka, Hideo; Morikawa, Osamu; Konishi, Hisatoshi
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 7 p. 1691 - 1697
反应条件
in acetone
7.5 h; Ambient temperatureIrradiation;
参考文献
Kobayashi; Shimizu; Sasaki; Suginome
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4614 - 4618
反应条件
1: 92 percent / CHCl3 / 5 h / Ambient temperature
2: 29 percent / acetonitrile / 1 h / Irradiation
View Scheme
参考文献
Hatzigrigoriou, Evangelia; Spyroudis, Spyros; Varvoglis, Anastasios
Liebigs Annalen der Chemie, 1989 , p. 167 - 170
反应条件
in acetone
30 h; Ambient temperatureIrradiation;
参考文献
Kobayashi; Shimizu; Sasaki; Suginome
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4614 - 4618
反应条件
1: 84 percent / Ac2O / 4 h / 20 - 100 °C
2: 87 percent / dimethylformamide / 2 h / 70 °C
View Scheme
参考文献
Rosenau, Thomas; Mereiter, Kurt; Jaeger, Christian; Schmid, Peter; Kosma, Paul
Tetrahedron, 2004 , vol. 60, # 27 p. 5719 - 5723