2-羟基-1,4-萘醌合成路线 （共 313 条）
参考文献
Research Corp.
Patent: US2553647 , 1946 ;
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Research Corp.
Patent: US2553648 , 1948 ;
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Du Pont de Nemours and Co.
Patent: US2572946 , 1949 ;
参考文献
Fieser et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 3177
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Fieser
Patent: US2398418 , 1943 ;
反应条件
1: ethanol
2: Zn, Py
View Scheme
参考文献
Porter,T.H. et al.
Journal of Medicinal Chemistry, 1973 , vol. 16, p. 115 - 118
反应条件
1: With ammonium cerium (IV) nitrate in acetonitrile
T=0 - 20°C;
2: With sulfuric acid in acetonitrile
T=20°C; 0.5 h;
参考文献
Ferreira, Sabrina Baptista; Kaiser, Carlos Roland; Ferreira, Vitor Francisco
Organic Preparations and Procedures International, 2009 , vol. 41, # 3 p. 211 - 215
反应条件
ammonium cerium (IV) nitrate in acetonitrile
T=0 - 20°C;
参考文献
Ferreira, Sabrina Baptista; Kaiser, Carlos Roland; Ferreira, Vitor Francisco
Organic Preparations and Procedures International, 2009 , vol. 41, # 3 p. 211 - 215
反应条件
1: 59 percent / potassium carbonate / dimethylformamide / 3 h / Heating
2: 61 percent / H2SO4 / CH2Cl2 / 0.75 h / 0 °C
View Scheme
参考文献
Kongkathip, Ngampong; Kongkathip, Boonsong; Siripong, Pongpun; Sangma, Chak; Luangkamin, Suwaporn; Niyomdecha, Momad; Pattanapa, Suppachai; Piyaviriyagul, Suratsawadee; Kongsaeree, Palangpon
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 14 p. 3179 - 3191
反应条件
acetic anhydride
T=20 - 100°C; 4 h;
参考文献
Rosenau, Thomas; Mereiter, Kurt; Jaeger, Christian; Schmid, Peter; Kosma, Paul
Tetrahedron, 2004 , vol. 60, # 27 p. 5719 - 5723
反应条件
1: 92 percent / CHCl3 / 5 h / Ambient temperature
2: 60 percent / acetic acid / 8 h / 40 - 50 °C
View Scheme
参考文献
Hatzigrigoriou, Evangelia; Spyroudis, Spyros; Varvoglis, Anastasios
Liebigs Annalen der Chemie, 1989 , p. 167 - 170
反应条件
formic acid in ethanol; water
T=200°C; P=155.149 - 155149 Torr; 3 h; chemoselective reaction;
参考文献
Ferreira, Sabrina Baptista; Rodriguesdarocha, David; Carneiro, Jose Walkimar M.; Santos, Wilson Costa; Ferreira, Vitor Francisco
Synlett, 2011 , # 11 p. 1551 - 1554
参考文献
Fieser
Patent: US2398418 , 1943 ;
