邻苯二甲酸二(二乙基酰胺)合成路线 （共 10 条）
反应条件
1,4-diaza-bicyclo[2.2.2]octane; benzenesulfonyl chloride in acetone
T=20 - 23°C; 0.0833333 h;
参考文献
Urbanski, Jerzy; Manek, Maria Beata
Polish Journal of Chemistry, 1983 , vol. 57, # 4/5/6 p. 603 - 605
反应条件
in hexane
Ambient temperature;
参考文献
Bowser, James R.; Williams, Pamela J.; Kurz, Kenneth
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 4111 - 4113
反应条件
1: 70 percent / SOCl2 / CHCl3 / 2 h / Heating
2: H2, quinoline, S / 10percent Pd/BaSO4 / xylene / Heating
View Scheme
参考文献
Mayer, Klaus K.; Poettinger, Theodor; Wiegrebe, Wolfgang
Archiv der Pharmazie (Weinheim, Germany), 1981 , vol. 314, # 8 p. 669 - 674
反应条件
quinoline; hydrogen; Pd-BaSO4 in xylene
Heating; Yield given;
参考文献
Mayer, Klaus K.; Poettinger, Theodor; Wiegrebe, Wolfgang
Archiv der Pharmazie (Weinheim, Germany), 1981 , vol. 314, # 8 p. 669 - 674
参考文献
Singh,S.N.; George,M.V.
Journal of Organic Chemistry, 1971 , vol. 36, p. 615 - 623
反应条件
1: diethyl ether
2: benzene / Heating
View Scheme
参考文献
Singh,S.N.; George,M.V.
Journal of Organic Chemistry, 1971 , vol. 36, p. 615 - 623
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium
1) THF, cyclohexane, -78 deg C, 1 h, 2) to room temperature, 12 h; Yield given. Multistep reaction;
参考文献
De Silva; Reed; Billedeau; Wang; Norris; Snieckus
Tetrahedron, 1992 , vol. 48, # 23 p. 4863 - 4878
参考文献
Maxim
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1927 , vol. 184, p. 690
Annales de Chimie (Cachan, France), 1928 , vol. <10> 9, p. 65,90
参考文献
Maxim
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1927 , vol. 184, p. 690
Annales de Chimie (Cachan, France), 1928 , vol. <10> 9, p. 65,90
参考文献
Maxim
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1927 , vol. 184, p. 690
Annales de Chimie (Cachan, France), 1928 , vol. <10> 9, p. 65,90
