1,2,3,4,6-alpha-D-葡萄糖五乙酸酯合成路线 (共 153 条)
反应条件
zinc(II) iodide in dichloromethane T=20°C; 2 h; Inert atmosphere;
参考文献
Tran, Anh-Tuan; Burden, Richard; Racys, Daugirdas T.; Carmen Galan
Chemical Communications, 2011 , vol. 47, # 15 p. 4526 - 4528
反应条件
1: glucose pentaacetate With boron trifluoride diethyl etherate in dichloromethane T=20°C; 1 h; 2: allyl alcohol in dichloromethane T=20°C; 4 h;
参考文献
Chemistry and Physics of Lipids, , vol. 114, # 2 p. 139 - 147
反应条件
tin(IV) chloride in dichloromethane Substitution;
参考文献
Gomez, Ana M.; Danelon, Gerardo O.; Valverde, Serafin; Lopez, J. Cristobal
Carbohydrate Research, 1999 , vol. 320, # 1-2 p. 138 - 142
反应条件
1: 99 percent / HBr; AcOH / CH2Cl2 / 0 - 20 °C 2: 68 percent / Ag2CO3; I2 / CH2Cl2 / 15 h / 20 °C View Scheme
参考文献
Sen, Asish K.; Banerji, Nilima
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 818 - 823
反应条件
boron trifluoride diethyl etherate
参考文献
Ikeda, Tsuyoshi; Miyashita, Hiroyuki; Kajimoto, Tetsuya; Nohara, Toshihiro
Tetrahedron Letters, 2001 , vol. 42, # 12 p. 2353 - 2356
反应条件
boron trifluoride diethyl etherate in dichloromethane T=20°C; 8 h;
参考文献
Dasgupta, Somnath; Rajput, Vishal Kumar; Roy, Bimalendu; Mukhopadhyay, Balaram
Journal of Carbohydrate Chemistry, 2007 , vol. 26, # 2 p. 91 - 106
反应条件
boron trifluoride diethyl etherate in dichloromethane T=20°C; 8 h;
参考文献
Dasgupta, Somnath; Rajput, Vishal Kumar; Roy, Bimalendu; Mukhopadhyay, Balaram
Journal of Carbohydrate Chemistry, 2007 , vol. 26, # 2 p. 91 - 106
反应条件
boron trifluoride diethyl etherate in dichloromethane 2 h; Heating;
参考文献
Sofia, Michael J.; Kakarla, Ramesh; Kogan, Natan; Dulina, Richard; Hui; Hatzenbuhler, Nicole T.; Liu, Dashan; Chen, Anna; Wagler, Thomas
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 17 p. 2251 - 2254
反应条件
zinc(II) iodide in dichloromethane T=20°C; 2 h; Inert atmosphere;
参考文献
Tran, Anh-Tuan; Burden, Richard; Racys, Daugirdas T.; Carmen Galan
Chemical Communications, 2011 , vol. 47, # 15 p. 4526 - 4528
反应条件
1: 2,3,4,6-tetra-OAc-D-manopyranose With hydrogen bromide in dichloromethane; acetic acid T=20°C; 1.5 h; 2: methanol in dichloromethane T=20°C; 12 h; Further stages.;
参考文献
Callam; Lowary
Journal of Organic Chemistry, 2001 , vol. 66, # 26 p. 8961 - 8972