反应条件
1: cyclododecane-1-one With lithium diisopropyl amide in tetrahydrofuran; hexane T=0°C; 0.5 h; 2: methyl iodide in tetrahydrofuran; hexane T=-78°C; 3: With 3-chloro-benzenecarboperoxoic acid in chloroform T=70°C; Baeyer-Villiger oxidation; 168000 h; Further stages. Title compound not separated from byproducts.;
参考文献
Van Buijtenen, Jeroen; Van As, Bart A. C.; Verbruggen, Marloes; Roumen, Luc; Vekemans, Jef A. J. M.; Pieterse, Koen; Hilbers, Peter A. J.; Hulshof, Lumbertus A.; Palmans, Anja R. A.; Meijer
Journal of the American Chemical Society, 2007 , vol. 129, # 23 p. 7393 - 7398