1: N,N-dimethyl acetamide / 0.17 h / 200 °C / |Sealed tube; |Microwave irradiation 2: sodium hydroxide View Scheme
参考文献
Moseley, Jonathan D.; Lenden, Philip; Lockwood, Mark; Ruda, Katinka; Sherlock, Jon-Paul; Thomson, Anthony D.; Gilday, John P.
Organic Process Research and Development, 2008 , vol. 12, # 1 p. 30 - 40
1: o-hydroxynitrobenzene With 1,4-diaza-bicyclo[2.2.2]octane in 1-methyl-pyrrolidin-2-one
T=50°C;
2: N,N-dimethylthiocarbamoyl chloride in 1-methyl-pyrrolidin-2-one
T=50°C; 2.5 h;
参考文献
Moseley, Jonathan D.; Lenden, Philip; Lockwood, Mark; Ruda, Katinka; Sherlock, Jon-Paul; Thomson, Anthony D.; Gilday, John P.
Organic Process Research and Development, 2008 , vol. 12, # 1 p. 30 - 40
