(E)-1-甲基-1,2二苯基乙烯合成路线 (共 175 条)
反应条件
sodium chlorite; (ethylenedinitrilo)tetraacetic acid disodium salt in water; acetonitrile T=55 - 65°C; 21 h;
参考文献
Geng, Xue-Li; Wang, Zhi; Li, Xiao-Qiang; Zhang, Chi
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9610 - 9613
参考文献
Shi, Yian
Patent: US6348608 B1, 2002 ;
Location in patent: Page column 31 ;
反应条件
Oxonereg;; ethylenediaminetetraacetic acid; sodium hydrogencarbonate; 1,2,4,5-di-O-isopropylidene-D-erythro-2,3-hexodiuro-2,6-pyranose in acetonitrile T=0°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bulman Page, Philip C.; Bartlett, Christopher J.; Chan, Yohan; Day, David; Parker, Phillip; Buckley, Benjamin R.; Rassias, Geracimos A.; Slawin, Alexandra M. Z.; Allin, Steven M.; Lacour, Jerome; Pinto, Andre
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 6128 - 6138
反应条件
2,3,5,6-tetramethylpyrazine N,N'-dioxide; [RuCl(C60H44N2O2)(NO)] in 1,4-dioxane T=20°C; 17.5 h; Irradiation; Title compound not separated from byproducts;
参考文献
Nakata, Kenya; Takeda, Tsuyoshi; Mihara, Jun; Hamada, Tetsuya; Irie, Ryo; Katsuki, Tsutomu
Chemistry - A European Journal, 2001 , vol. 7, # 17 p. 3776 - 3782
反应条件
iodine in hexane T=40°C; Sealed tubeIrradiation;
参考文献
Chen, Ying-Zhe; Ni, Ching-Wen; Teng, Fu-Lin; Ding, Yi-Shun; Lee, Tunng-Hsien; Ho, Jinn-Hsuan
Tetrahedron, 2014 , vol. 70, # 9 p. 1748 - 1762
反应条件
hydrogen bromide in acetic acid
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 183 - 194
反应条件
1: iodine / hexane / 40 °C / |Sealed tube; |Irradiation 2: N-bromosuccinmide; dibenzoyl peroxide / ethyl acetate / 2 h / |Reflux View Scheme
参考文献
Chen, Ying-Zhe; Ni, Ching-Wen; Teng, Fu-Lin; Ding, Yi-Shun; Lee, Tunng-Hsien; Ho, Jinn-Hsuan
Tetrahedron, 2014 , vol. 70, # 9 p. 1748 - 1762
反应条件
Behandlung des Reaktionsprodukts mit wss. AgNO3-Loesung; 1.2-diphenyl-propene-(1);
参考文献
Tiffeneau; Levy
Bulletin de la Societe Chimique de France, 1931 , vol. <4> 49, p. 1806,1811
反应条件
2,3,5,6-tetramethylpyrazine N,N'-dioxide; [RuCl(C60H44N2O2)(NO)] in 1,4-dioxane
T=20°C; 17.5 h; Irradiation; Title compound not separated from byproducts;
参考文献
Nakata, Kenya; Takeda, Tsuyoshi; Mihara, Jun; Hamada, Tetsuya; Irie, Ryo; Katsuki, Tsutomu
Chemistry - A European Journal, 2001 , vol. 7, # 17 p. 3776 - 3782
参考文献
Schmitt; Suquet
Bulletin de la Societe Chimique de France, 1955 , p. 84,86