(E)-1-甲基-1,2二苯基乙烯合成路线 （共 175 条）
反应条件
1: in diethyl ether; toluene T=-40 - 20°C; 2: With water Title compound not separated from byproducts;
参考文献
European Journal of Organic Chemistry, , # 6 p. 993 - 997
反应条件
hydrogenchloride in diethyl ether; water under Ar, excess dild. HCl, 20 h; separation of the phases, the upper is dried with Na2SO4, removal of solvent, recrystn. (methanol);
参考文献
Klein, Hans-Friedrich; Reitzel, Lutz
Chemische Berichte, 1988 , vol. 121, p. 1115 - 1118
反应条件
methylethyl sulfide; palladium diacetate; silver carbonate; 2,2,2-trimethylacetic acid T=120°C; Heck type coupling reaction; 8 h; Inert atmosphere;
参考文献
Li, Hu; He, Ke-Han; Liu, Jia; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Shi, Zhang-Jie
Chemical Communications, 2012 , vol. 48, # 56 p. 7028 - 7030
反应条件
1: acetic acid; lithium chloride / 24 h / 25 °C 2: palladium diacetate; triphenylphosphine; caesium carbonate / tetrahydrofuran / 5 h / 40 °C / |Inert atmosphere 3: NiCl2(PPh3)2 / tetrahydrofuran / 12 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 13 p. 2175 - 2185
反应条件
ethanol; sodium ethanolate
参考文献
Journal of the American Chemical Society, , vol. 78, p. 790,792, 793
反应条件
sodium acetate; bis(dibenzylideneacetone)-palladium(0) in dichloromethane 2 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 37, p. 31 - 36
反应条件
palladium diacetate in acetonitrile T=25°C; 72 h; Yields of byproduct given;
参考文献
Matoba, Kazutaka; Motofusa, Shin-Ichi; Sik Cho, Chan; Ohe, Kouichi; Uemura, Sakae
Journal of Organometallic Chemistry, 1999 , vol. 574, # 1 p. 3 - 10
反应条件
1: diethyl ether 2: ethanolic KOH 3: glacial acetic acid; HBr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 55, p. 2960,2965
反应条件
1: ethanolic KOH 2: glacial acetic acid; HBr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 55, p. 2960,2965
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene 16 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 12 p. 4035 - 4042
