4 -甲氧基二苯基甲烷合成路线 （共 196 条）
反应条件
digallium tetrachloride in carbon disulfide
24 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Hashimoto, Yukihiko; Hirata, Kazujuki; Kagoshima, Hirotaka; Kihara, Nobuhiro; Hasegawa, Masaki; Saigo, Kazuhiko
Tetrahedron, 1993 , vol. 49, # 27 p. 5969 - 5978
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h
1.2: 2 h
2.1: copper(l) iodide / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere
View Scheme
参考文献
Li, Man-Bo; Tang, Xiang-Ling; Tian, Shi-Kai
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1980 - 1984
反应条件
1: magnesium / diethyl ether / 0.5 h / |Inert atmosphere; |Schlenk technique
2: tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; lithium chloride / N,N-dimethyl-formamide / 12 h / 20 °C / |Sonication; |Inert atmosphere
View Scheme
参考文献
Ocampo, Romina A.; Koll, Liliana C.; Mandolesi, Sandra D.
Ultrasonics Sonochemistry, 2013 , vol. 20, # 1 p. 40 - 46
反应条件
1: zinc; ammonium chloride / tetrahydrofuran; water / 24 h / 20 °C / |Reflux
2: tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; lithium chloride / N,N-dimethyl-formamide / 12 h / 20 °C / |Sonication; |Inert atmosphere
View Scheme
参考文献
Ocampo, Romina A.; Koll, Liliana C.; Mandolesi, Sandra D.
Ultrasonics Sonochemistry, 2013 , vol. 20, # 1 p. 40 - 46
反应条件
1: zinc; ammonium chloride / benzene; diethyl ether / 12 h / 0 °C / |Reflux; |Inert atmosphere
2: tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; lithium chloride / N,N-dimethyl-formamide / 12 h / 20 °C / |Sonication; |Inert atmosphere
View Scheme
参考文献
Ocampo, Romina A.; Koll, Liliana C.; Mandolesi, Sandra D.
Ultrasonics Sonochemistry, 2013 , vol. 20, # 1 p. 40 - 46
反应条件
1: diethyl ether / 0.25 h / 0 °C
2: bis(1,5-cyclooctadiene)nickel (0); diphenylcyclohexyl phosphine; cesium fluoride / 1,4-dioxane / 24 h / 40 °C / |Inert atmosphere; |Glovebox
View Scheme
参考文献
Maity, Prantik; Shacklady-Mcatee, Danielle M.; Yap, Glenn P. A.; Sirianni, Eric R.; Watson, Mary P.
Journal of the American Chemical Society, 2013 , vol. 135, # 1 p. 280 - 285
反应条件
1: diethyl ether
2: hypophosphorous acid; iodine / acetic acid / 60 °C
View Scheme
参考文献
Meng, Li; Su, Jihu; Zha, Zhenggen; Zhang, Li; Zhang, Zhenlei; Wang, Zhiyong
Chemistry - A European Journal, 2013 , vol. 19, # 18 p. 5542 - 5545
反应条件
hydrogenchloride; zinc(II) chloride
T=100°C;
参考文献
Short; Stewart
Journal of the Chemical Society, 1929 , p. 559
反应条件
hydrogenchloride; zinc(II) chloride
T=100°C; Versetzen des Reaktionsprodukts mit Benzylchlorid;
参考文献
Short; Stewart
Journal of the Chemical Society, 1929 , p. 559
反应条件
aluminium trichloride in n-heptane
time, solvent and temperature dependence of isomerization; Product distribution;
参考文献
Olah, George A.; Olah, Judith A.; Ohyama, Toshiyuki
Journal of the American Chemical Society, 1984 , vol. 106, # 18 p. 5284 - 5290
