4 -甲氧基二苯基甲烷合成路线 (共 196 条)
反应条件
palladium diacetate; potassium hexamethylsilazane; Nixantphos in tetrahydrofuran
T=24°C; 12 h; Inert atmosphere;
参考文献
Zhang, Jiadi; Bellomo, Ana; Trongsiriwat, Nisalak; Jia, Tiezheng; Carroll, Patrick J.; Dreher, Spencer D.; Tudge, Matthew T.; Yin, Haolin; Robinson, Jerome R.; Schelter, Eric J.; Walsh, Patrick J.
Journal of the American Chemical Society, 2014 , vol. 136, # 17 p. 6276 - 6287
反应条件
water; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride
T=60°C; 5 h; regioselective reaction;
参考文献
Qin, Chong; Shen, Tao; Tang, Conghui; Jiao, Ning
Angewandte Chemie - International Edition, 2012 , vol. 51, # 28 p. 6971 - 6975
反应条件
titanium tetrachloride in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Li, Hui-Jing; Guillot, Regis; Gandon, Vincent
Journal of Organic Chemistry, 2010 , vol. 75, # 24 p. 8435 - 8449
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane
T=60°C; 24 h;
参考文献
Lemaire, Marc; Doussot, Joel; Guy, Alain
Chemistry Letters, 1988 , # 10 p. 1581 - 1584
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,2-dichloro-ethane
T=100°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Yi, Hong; Liu, Qiang; Liu, Jie; Zeng, Ziqi; Yang, Yuhong; Lei, Aiwen
ChemSusChem, 2012 , vol. 5, # 11 p. 2143 - 2146
参考文献
Short; Stewart
Journal of the Chemical Society, 1929 , p. 559