4 -甲氧基二苯基甲烷合成路线 （共 196 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; lithium chloride in tetrahydrofuran; N,N-dimethyl-formamide
T=80°C; 22 h;
参考文献
Curran, Dennis P.; Hoshino, Masahide
Journal of Organic Chemistry, 1996 , vol. 61, # 19 p. 6480 - 6481
反应条件
NaBEt3H; iron(II) chloride in tetrahydrofuran
1.) -78 deg C, 10 min., 2.) room temp.;
参考文献
Alper, Howard; Ripley, Sharon; Prince, Trish L.
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 250 - 252
反应条件
Trimethylene glycol; scandium tris(trifluoromethanesulfonate) in 1,2-dichloro-ethane
Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tsuchimoto, Teruhisa; Hiyama, Tamejiro; Fukuzawa, Shin-Ichi
Chemical Communications, 1996 , # 20 p. 2345 - 2346
反应条件
[Msim]AlCl4
T=70°C; 1 h; SolventTemperatureTimeReagent/catalyst;
参考文献
Zolfigol, Mohammad Ali; Vahedi, Hooshang; Azimi, Saeid; Moosavi-Zare, Ahmad Reza
Synlett, 2013 , vol. 24, # 9 art. no. ST-2013-D0110-L, p. 1113 - 1116
反应条件
sodium hydroxide; dicobalt octacarbonyl; tetra(n-butyl)ammonium hydrogensulfate in water; benzene
T=60°C; 16 h; with triiron dodecarbonyl; Yield given;
参考文献
Alper, Howard; Sibtain, Fazle; Heveling, Josef
Tetrahedron Letters, 1983 , vol. 24, # 48 p. 5329 - 5332
反应条件
(C6H5CON2C3H(CF3)2O)Ni(II)(tris(4-dimethylamino)pyridine) in tetrahydrofuran
T=70°C; 24 h; Inert atmosphere;
参考文献
Someya, Chika I.; Inoue, Shigeyoshi; Krackl, Sebastian; Irran, Elisabeth; Enthaler, Stephan
European Journal of Inorganic Chemistry, 2012 , # 8 p. 1269 - 1277
反应条件
(CH3CON2C3H(CF3)2O)Ni(II)(tris(4-dimethylamino)pyridine) in tetrahydrofuran
T=70°C; 24 h; Inert atmosphere;
参考文献
Someya, Chika I.; Inoue, Shigeyoshi; Krackl, Sebastian; Irran, Elisabeth; Enthaler, Stephan
European Journal of Inorganic Chemistry, 2012 , # 8 p. 1269 - 1277
反应条件
(C6H5CON2C3H(CF3)2O)Ni(II)(tris(4-dimethylamino)pyridine) in tetrahydrofuran
T=70°C; 24 h; Inert atmosphere;
参考文献
Someya, Chika I.; Inoue, Shigeyoshi; Krackl, Sebastian; Irran, Elisabeth; Enthaler, Stephan
European Journal of Inorganic Chemistry, 2012 , # 8 p. 1269 - 1277
反应条件
FeCl(THF)L1 in diethyl ether
T=20°C; 0.5 h; Schlenk techniqueInert atmosphere; Catalytic behavior;
参考文献
UNIVERSITY OF PRINCE EDWARD ISLAND; GENESIS GROUP INC.; SHAVER, Michael, P.; KOZAK, Christopher, M.
Patent: WO2013/53046 A1, 2013 ;
Location in patent: Paragraph 00282-00284 ;
反应条件
scandium tris(trifluoromethanesulfonate)
T=120°C; Friedel-Crafts benzylation reaction; 0.5 h;
参考文献
Mukaiyama, Teruaki; Kamiyama, Hiroaki; Yamanaka, Hiroyuki
Chemistry Letters, 2003 , vol. 32, # 9 p. 814 - 815
