N-(2-溴甲基吡啶-6-基)邻苯二甲酰亚胺合成路线 (共 6 条)
反应条件
1: NaI / ethanol / 15 h / Heating 2: hydrazine hydrate View Scheme
参考文献
Goswami; Ghosh; Mukherjee; Avijit Kumar Adak; Ajit Kumar Mahapatra
Journal of Heterocyclic Chemistry, 2001 , vol. 38, # 1 p. 173 - 178
反应条件
N-bromosuccinmide in tetrachloromethane; water
参考文献
Goswami; Ghosh; Mukherjee; Avijit Kumar Adak; Ajit Kumar Mahapatra
Journal of Heterocyclic Chemistry, 2001 , vol. 38, # 1 p. 173 - 178
反应条件
dibenzoyl peroxide in tetrachloromethane
参考文献
Merck and Co., Inc.
Patent: US4490533 A1, 1984 ;
反应条件
1: 95 percent / 1 h / 190 °C
2: N-bromosuccinimide; AIBN / benzene / 5 h / Heating
View Scheme
参考文献
Congreve, Miles; Aharony, David; Albert, Jeffrey; Callaghan, Owen; Campbell, James; Carr, Robin A. E.; Chessari, Gianni; Cowan, Suzanna; Edwards, Philip D.; Frederickson, Martyn; McMenamin, Rachel; Murray, Christopher W.; Patel, Sahil; Wallis, Nicola
Journal of Medicinal Chemistry, 2007 , vol. 50, # 6 p. 1124 - 1132
反应条件
1: 95 percent / 1 h / 190 °C
2: N-bromosuccinimide; AIBN / benzene / 5 h / Heating
View Scheme
参考文献
Congreve, Miles; Aharony, David; Albert, Jeffrey; Callaghan, Owen; Campbell, James; Carr, Robin A. E.; Chessari, Gianni; Cowan, Suzanna; Edwards, Philip D.; Frederickson, Martyn; McMenamin, Rachel; Murray, Christopher W.; Patel, Sahil; Wallis, Nicola
Journal of Medicinal Chemistry, 2007 , vol. 50, # 6 p. 1124 - 1132
反应条件
N-bromosuccinmide
0.15 h; microwave irradiation;
参考文献
Goswami, Shyamaprosad; Dey, Swapan; Jana, Subrata; Adak, Avijit Kumar
Chemistry Letters, 2004 , vol. 33, # 7 p. 916 - 917