Hennen, William J.; Hinshaw, Barbara C.; Riley, Timothy A.; Wood, Steven G.; Robins, Roland K.
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1741 - 1746
1: 100 percent / Dowex 50W-X8(H+), H2Se(gas) / methanol / 1 h / -22 °C
2: 17 percent / methanol / 0.5 h
3: 40 percent / concd. HCl, 50percent aq. hypophosphorus acid, NaNO2 / H2O / 1 h / 0 °C
4: 87 percent / NH3(gas) / methanol / 24 h / 22 °C
View Scheme
参考文献
Hennen, William J.; Hinshaw, Barbara C.; Riley, Timothy A.; Wood, Steven G.; Robins, Roland K.
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1741 - 1746
1: 17 percent / methanol / 0.5 h
2: 40 percent / concd. HCl, 50percent aq. hypophosphorus acid, NaNO2 / H2O / 1 h / 0 °C
3: 87 percent / NH3(gas) / methanol / 24 h / 22 °C
View Scheme
参考文献
Hennen, William J.; Hinshaw, Barbara C.; Riley, Timothy A.; Wood, Steven G.; Robins, Roland K.
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1741 - 1746
1: 40 percent / concd. HCl, 50percent aq. hypophosphorus acid, NaNO2 / H2O / 1 h / 0 °C
2: 87 percent / NH3(gas) / methanol / 24 h / 22 °C
View Scheme
参考文献
Hennen, William J.; Hinshaw, Barbara C.; Riley, Timothy A.; Wood, Steven G.; Robins, Roland K.
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1741 - 1746