1: triethylamine; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 2 h / 0 °C / |Inert atmosphere
2: (Ph)2SiH2; P-(phenyl)dibenzophosphole / 1,4-dioxane / 24 h / 101 °C / |Inert atmosphere
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参考文献
Van Kalkeren, Henri A.; Te Grotenhuis, Colet; Haasjes, Frank S.; Hommersom; Rutjes, Floris P. J. T.; Van Delft, Floris L.
European Journal of Organic Chemistry, 2013 , # 31 p. 7059 - 7066
1: hydrazine / methanol; chloroform; water / 12 h / 20 °C
2: acetic acid / water / 0.5 h / 20 °C
3: oxygen; copper(II) bis(trifluoromethanesulfonate) / toluene / 3.5 h / 80 °C
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