反应条件
tetrafluoroboric acid diethyl ether complex; potassium fluoride; lt;(CpTMS)2YMegt;2; SiMePh; dihydrogen peroxide; potassium hydrogencarbonate
1.) cyclohexane, room temperature, 12 h, 2.) CHCl3, 0 deg C, 1 h, 3.) MeOH, THF, reflux, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Molander, Gary A.; Dowdy, Eric D.; Schumann, Herbert
Journal of Organic Chemistry, 1998 , vol. 63, # 10 p. 3386 - 3396