1-(2,4-二硝基苯基)哌啶合成路线 (共 93 条)
反应条件
dihydrogen peroxide in formic acid 36 h; Ambient temperature;
参考文献
Khuthier, Abdul-Hussain; Al-Mallah, Khawla Y.; Hanna, Salim Y.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 109 - 112
反应条件
dihydrogen peroxide in formic acid
参考文献
Al-Kazzaz, Abdul-Khalik S.; Hanna, Salim Y.; Khuthier, Abdul-Hussain
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1661 - 1664
参考文献
Archiv der Pharmazie, , vol. 315, # 4 p. 333 - 339
反应条件
sodium sulfide; ethanol; sulfur Reagens 4: Wasser;
参考文献
Saunders
Journal of the Chemical Society, 1955 , p. 3275,3282
反应条件
ammonium hydroxide in methanol T=70°C; 12 h;
参考文献
Forlani, Luciano; Boga, Carla; Mazza, Milena; Cavrini, Vanni; Andrisano, Vincenza
Tetrahedron, 1998 , vol. 54, # 18 p. 4647 - 4654
反应条件
sulfuric acid in water T=25°C; var. hydroxide ion concentration and on amine concentration; Rate constant;
参考文献
Vargas, Elba B. de; Rossi, Rita H. de; Veglia, Alicia V.
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 1976 - 1981
反应条件
sodium hydroxide in 1,4-dioxane; water T=25°C; ionic strength μ= 1 M (NaCl), in the presence or absenece of piperidine, variation of concentrations of base and amine; Rate constant;
参考文献
Gierczyk; Leska; Nowak-Wydra; Schroeder; Wojciechowski; Bartl; Brzezinski
Journal of Molecular Structure, 2000 , vol. 524, # 1-3 p. 217 - 225
反应条件
sulfuric acid in water T=25°C; var. hydroxide ion concentration and on amine concentration; Rate constant;
参考文献
Vargas, Elba B. de; Rossi, Rita H. de; Veglia, Alicia V.
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 1976 - 1981
反应条件
in dimethyl sulfoxide T=50°C; 2 h;
参考文献
Sekiguchi, Shizen; Ishikura, Hiromi; Hirosawa, Yukitoshi; Ono, Nobuyuki
Tetrahedron, 1990 , vol. 46, # 16 p. 5567 - 5578
反应条件
in acetonitrile
T=20°C; 0.366667 h;
参考文献
Liguori, Lucia; Bjorsvik, Hans-Rene
Organic Process Research and Development, 2011 , vol. 15, # 5 p. 997 - 1009