反式-2-苯乙烯硼酸频哪酸酯合成路线 (共 45 条)
反应条件
sodium azide; copper(II) sulfate in methanol
T=20°C; 4 h; Inert atmosphere;
参考文献
Hemelaere, Remy; Caijo, Frederic; Mauduit, Marc; Carreaux, Francois; Carboni, Bertrand
European Journal of Organic Chemistry, 2014 , vol. 2014, # 16 p. 3328 - 3333
反应条件
copper diacetate; dichlorobis(trimethylphosphite)palladium(II) in N,N-dimethyl-formamide
T=87°C; Mizoroki-Heck type reaction; 24 h;
参考文献
Du, Xiaoli; Suguro, Masahiro; Hirabayashi, Kazunori; Mori, Atsunori; Nishikata, Takashi; Hagiwara, Nobuhito; Kawata, Kentaro; Okeda, Takeaki; Wang, Hui Feng; Fugami, Keigo; Kosugi, Masanori
Organic Letters, 2001 , vol. 3, # 21 p. 3313 - 3316
反应条件
copper (II) acetate monohydrate; lithium tert-butylate; triethyl phosphite in tetrahydrofuran
T=20°C; Inert atmosphereSchlenk technique;
参考文献
Sakae, Ryosuke; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Chemistry Letters, 2013 , vol. 42, # 10 p. 1128 - 1130
反应条件
N-bromosuccinmide; Schwartz's reagent; copper(I) bromide dimethylsulfide complex
1.) CH2Cl2, r.t.; 2.) CH2Cl2, r.t., 30 min; Yield given. Multistep reaction;
参考文献
Zheng, Bin; Srebnik, Morris
Tetrahedron Letters, 1995 , vol. 36, # 32 p. 5665 - 5668
反应条件
tetrakis(triphenylphosphine) palladium(0); water; sodium carbonate in ethanol; toluene
T=100°C; Suzuki coupling; 17 h;
参考文献
Bagwell, Claire L.; Moloney, Mark G.; Thompson, Amber L.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 14 p. 4081 - 4086