2,3-二氯-5,6-二氰基-1,4-苯醌合成路线 (共 141 条)
反应条件
in acetonitrile T=25°C; Equilibrium constant;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 9 p. 2673 - 2674
反应条件
pyridine; chlorosulfonic acid; copper Reagens 4: Nickel-Aluminium-Legierung; Reagens 5: wss. NaOH; Reagens 6: Benzol; Reaktion ueber mehrere Stufen;
参考文献
Desai; Venkataraman
Tetrahedron, 1959 , vol. 5, p. 305,308
反应条件
sodium hydroxide in 1,4-dioxane; ethyl acetate; Petroleum ether
参考文献
Synthelabo
Patent: US6063810 A1, 2000 ;
反应条件
copper diacetate; silver(l) oxide in 1-methyl-pyrrolidin-2-one T=120°C; 20 h;
参考文献
Zheng, Kui; Yu, Peng; Chen, Shuyou; Chen, Fen; Cheng, Jiang
Chinese Journal of Chemistry, 2013 , vol. 31, # 4 p. 449 - 452
反应条件
in 1,4-dioxane 0.25 h; Ambient temperatureother primary and secondary aryl-substituted alcohols were also subject of study (Tab. I-IV);
参考文献
Journal of Organic Chemistry, , vol. 45, # 9 p. 1596 - 1600
反应条件
in ethanol on react. of methyl cobalamine with soln. of 2,3-dichloro-5,6-dicyano-benzoquinone-(1,4) at darkness, 30min;;
参考文献
Dolphin, D.; Johnson, A. W.; Rodrigo, R.
Journal of the Chemical Society, 1964 , p. 3186 - 3193
Full Text Show Details
Gmelin Handbook: Co: Org.Verb.1, 1.1.2.2, page 46 - 51
反应条件
copper diacetate; silver(l) oxide in 1-methyl-pyrrolidin-2-one T=120°C; 20 h;
参考文献
Zheng, Kui; Yu, Peng; Chen, Shuyou; Chen, Fen; Cheng, Jiang
Chinese Journal of Chemistry, 2013 , vol. 31, # 4 p. 449 - 452
反应条件
Ag2CO3; copper(II) bis(trifluoromethanesulfonate); potassium carbonate in N,N-dimethyl-formamide T=100°C; 20 h;
参考文献
Zhang, Guangyou; Chen, Shuyou; Fei, Haiyang; Cheng, Jiang; Chen, Fan
Synlett, 2012 , vol. 23, # 15 p. 2247 - 2250
反应条件
in acetonitrile stirring of a soln. of the compd. with DDQ in CH3CN (room temp., 30 min); filtration (sintered glass filter), evapn. to dryness, redissolving of the residue in CH2Cl2, chromy. (alumina column, CH2Cl2), removal of solvent;
参考文献
Lee, C. C.; Zhang, C. H.; Abd-El-Aziz, A. S.; Piorko, A.; Sutherland, R. G.
Journal of Organometallic Chemistry, 1989 , vol. 364, p. 217 - 230
参考文献
Linstead et al.
Chemistry and Industry (London, United Kingdom), 1954 , p. 1174