2,6-二溴-1,5-二羟基萘合成路线 (共 7 条)
反应条件
1: With iodine in acetic acid T=80°C; Inert atmosphere; 2: With bromine in acetic acid 12 h; Reflux;
参考文献
US2011/224445 A1, ;
Page/Page column 19 ;
参考文献
Journal of the Chemical Society, , p. 236,239
Journal of the American Chemical Society, , vol. 52, p. 4872,4878
反应条件
1: 1,5-dihydroxy-2,6-dibromonaphthalene With sodium hydride in 1-methyl-pyrrolidin-2-one; mineral oil T=0°C; 0.0833333 h; Inert atmosphere; 2: methyl iodide in 1-methyl-pyrrolidin-2-one; mineral oil T=0 - 20°C;
参考文献
Macromolecules, , vol. 46, # 3 p. 718 - 726
反应条件
sodium hydroxide T=60°C;
参考文献
Journal of the Chemical Society, , p. 236,239
Journal of the American Chemical Society, , vol. 52, p. 4872,4878
反应条件
sodium hydroxide T=60°C;
参考文献
Journal of the Chemical Society, , p. 236,239
反应条件
sodium in ethanol 5 h; Heating;
参考文献
Segura, Jose L.; Martin, Nazario; Hanack, Michael
European Journal of Organic Chemistry, 1999 , # 3 p. 643 - 651
反应条件
ueber 2,6-Dibrom-8-nitro-naphthalin-1,5-diol und 8-Amino-2,6-dibrom-naphthalin-1,5-diol;
参考文献
Sandoz
Patent: US2623872 , 1949 ;