bromine in dichloromethane; N,N-dimethyl-formamide
T=58°C; 3 h;
参考文献
Musatova, I. S.; Elina, A. S.; Padeiskaya, E. N.; Shipilova, L. D.; Yakobson, G. G.; Furin, G. G.
Pharmaceutical Chemistry Journal, 1982 , vol. 16, # 8 p. 598 - 601
Khimiko-Farmatsevticheskii Zhurnal, 1982 , vol. 16, # 8 p. 934 - 938
1: 94.6 percent / butyl amine / 20 h / 20 - 25 °C
2: 99 percent / Br2 / CH2Cl2; dimethylformamide / 3 h / 58 °C
View Scheme
参考文献
Musatova, I. S.; Elina, A. S.; Padeiskaya, E. N.; Shipilova, L. D.; Yakobson, G. G.; Furin, G. G.
Pharmaceutical Chemistry Journal, 1982 , vol. 16, # 8 p. 598 - 601
Khimiko-Farmatsevticheskii Zhurnal, 1982 , vol. 16, # 8 p. 934 - 938
Musatova, I. S.; Elina, A. S.; Padeiskaya, E. N.; Shipilova, L. D.; Yakobson, G. G.; Furin, G. G.
Pharmaceutical Chemistry Journal, 1982 , vol. 16, # 8 p. 598 - 601
Khimiko-Farmatsevticheskii Zhurnal, 1982 , vol. 16, # 8 p. 934 - 938
1: 54.7 percent / Et3N / acetone / 0.5 h / Heating
2: 63 percent / NaOH / methanol / 0.75 h / 20 - 22 °C
View Scheme
参考文献
Musatova, I. S.; Elina, A. S.; Padeiskaya, E. N.; Shipilova, L. D.; Yakobson, G. G.; Furin, G. G.
Pharmaceutical Chemistry Journal, 1982 , vol. 16, # 8 p. 598 - 601
Khimiko-Farmatsevticheskii Zhurnal, 1982 , vol. 16, # 8 p. 934 - 938
