4-乙酰氧基-4'-溴代联苯合成路线 （共 21 条）
反应条件
bromine; sodium carbonate in 1,2-dichloro-ethane T=50°C;
参考文献
Zang, Zhi-Qian; Zhang, Dong; Wan, Xin-Hua; Zhou, Qi-Feng
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2000 , vol. 339, p. 145 - 158
参考文献
Journal of the American Chemical Society, , vol. 61, p. 3037
反应条件
1: 86 percent / Sulfuric acid / 3 h / 60 °C 2: 84.6 percent / Na2CO3; Br2 / 1,2-dichloro-ethane / 50 °C View Scheme
参考文献
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, , vol. 339, p. 145 - 158
反应条件
bromine; acetic acid
参考文献
Journal of the Chemical Society, , p. 3243
参考文献
Pr. Louisiana Acad. Sci., , vol. 10, p. 205
参考文献
Journal of the Chemical Society, , p. 3243
反应条件
1: KOH / ethanol 2: K2CO3 / acetone 3: Mg, C2H5Br / diethyl ether 4: 48percent HBr / acetic acid 5: H(+) / toluene View Scheme
参考文献
Surendranath, V.; Fishel, D. L.; Vries, A de; Mahmood, R.; Johnson, D. L.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 131, p. 1 - 8
反应条件
sodium hydroxide in ethanol; water 6 h; Heating;
参考文献
Zang, Zhi-Qian; Zhang, Dong; Wan, Xin-Hua; Zhou, Qi-Feng
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2000 , vol. 339, p. 145 - 158
反应条件
1.1: 83.8 percent / NaOH / H2O; ethanol / 6 h / Heating 2.1: sodium hydroxide / ethanol; H2O / Heating 3.1: n-BuLi / tetrahydrofuran; hexane / -78 - -65 °C 3.2: B(OCH3)3 / tetrahydrofuran; hexane / -65 - 20 °C 3.3: aq. HCl / tetrahydrofuran; hexane / 20 °C View Scheme
参考文献
Zang, Zhi-Qian; Zhang, Dong; Wan, Xin-Hua; Zhou, Qi-Feng
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2000 , vol. 339, p. 145 - 158
反应条件
1: 83.8 percent / NaOH / H2O; ethanol / 6 h / Heating 2: sodium hydroxide / ethanol; H2O / Heating View Scheme
参考文献
Surendranath, V.; Fishel, D. L.; Vries, A de; Mahmood, R.; Johnson, D. L.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 131, p. 1 - 8
