hydrogenchloride in tetrahydrofuran Cp2TiCH2SC6H4 dissolved in dry de-gassed THF at room temp., dry HCl gasbubbled through soln. for 2 min; evapd. in vac., heated at 0.1 mmHg to 130°C in short path distn.app., residue washed with pentane and ether;

hydrogenchloride in tetrahydrofuran Cp2TiCH2SC6H4 dissolved in dry de-gassed THF at room temp., dry HCl gasbubbled through soln. for 2 min; evapd. in vac., heated at 0.1 mmHg to 130°C in short path distn.app., residue washed with pentane and ether;