3-溴-4-N,N-二甲氨基吡啶合成路线 （共 7 条）
反应条件
bromine; potassium carbonate in tetrachloromethane 6 h;
参考文献
Paudler, William W.; Jovanovic, Misa V.
Journal of Organic Chemistry, 1983 , vol. 48, # 7 p. 1064 - 1069
反应条件
bromine; potassium carbonate in tetrachloromethane 6 h;
参考文献
Journal of Organic Chemistry, , vol. 48, # 7 p. 1064 - 1069
反应条件
phosphorus pentabromide in chloroform T=10°C; Inert atmosphere;
参考文献
Bezgubenko; Pipko; Sinitsa
Russian Journal of General Chemistry, 2009 , vol. 79, # 5 p. 911 - 918
参考文献
Bezgubenko; Pipko; Sinitsa
Russian Journal of General Chemistry, 2009 , vol. 79, # 5 p. 911 - 918
反应条件
KNH2 in diethyl ether; ammonia T=-78 - -33°C; 1.5 h;
参考文献
Heterocycles, , vol. 26, # 11 p. 2905 - 2910
反应条件
KNH2 in diethyl ether; ammonia T=-78°C; 0.0833333 h;
参考文献
Heterocycles, , vol. 26, # 11 p. 2905 - 2910
反应条件
1: (3-bromopyridin-4-yl)-dimethyl-amine With isopropylmagnesium chloride in tetrahydrofuran
T=20°C; 3 h;
2: p-toluenesulphonyl cyanide in tetrahydrofuran
参考文献
Poisson, Thomas; Oudeyer, Sylvain; Levacher, Vincent
Tetrahedron Letters, 2012 , vol. 53, # 26 p. 3284 - 3287
