3-烯丙基-2-(烯丙氧基)苯甲醛合成路线 （共 10 条）
反应条件
1: 57 percent / [RuClH(CO)(PPh3)3] / CH2Cl2 / 14 h / 65 °C 2: 70 percent / ((Mes)2C3H5N2)Cl2Ru=CHPh / toluene / 3 h / 90 °C View Scheme
参考文献
Van Otterlo, Willem A.L.; Morgans, Garreth L.; Madeley, Lee G.; Kuzvidza, Samuel; Moleele, Simon S.; Thornton, Natalie; De Koning, Charles B.
Tetrahedron, 2005 , vol. 61, # 32 p. 7746 - 7755
反应条件
0.166667 h; Neat (no solvent)Microwave irradiation;
参考文献
THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS
Patent: WO2008/134474 A2, 2008 ;
Location in patent: Page/Page column 70 ;
参考文献
Claisen; Eisleb
Justus Liebigs Annalen der Chemie, 1913 , vol. 401, p. 44
参考文献
Claisen; Eisleb
Justus Liebigs Annalen der Chemie, 1913 , vol. 401, p. 44
参考文献
Claisen; Eisleb
Justus Liebigs Annalen der Chemie, 1913 , vol. 401, p. 44
反应条件
potassium carbonate in methanol; water
参考文献
THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS
Patent: WO2008/134474 A2, 2008 ;
Location in patent: Page/Page column 70 ;
反应条件
1: microwave irradiation
2: 77 percent / K2CO3 / acetone / 2 h / 60 °C
View Scheme
参考文献
Van Otterlo, Willem A.L.; Morgans, Garreth L.; Madeley, Lee G.; Kuzvidza, Samuel; Moleele, Simon S.; Thornton, Natalie; De Koning, Charles B.
Tetrahedron, 2005 , vol. 61, # 32 p. 7746 - 7755
反应条件
1: K2CO3 / acetone
2: microwave irradiation
3: 77 percent / K2CO3 / acetone / 2 h / 60 °C
View Scheme
参考文献
Van Otterlo, Willem A.L.; Morgans, Garreth L.; Madeley, Lee G.; Kuzvidza, Samuel; Moleele, Simon S.; Thornton, Natalie; De Koning, Charles B.
Tetrahedron, 2005 , vol. 61, # 32 p. 7746 - 7755
反应条件
ethanol; potassium carbonate
参考文献
Claisen; Eisleb
Justus Liebigs Annalen der Chemie, 1913 , vol. 401, p. 44
反应条件
1: potassium carbonate
2: decalin / Reflux
3: potassium carbonate
View Scheme
参考文献
Chang, Meng-Yang; Lee, Nien-Chia
Synlett, 2012 , vol. 23, # 6 art. no. ST-2011-W0792-L, p. 867 - 872
