Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mulder, Patrick P. J.; Boere, Ben B.; Baart, Arthur; Cornelisse, Jan; Lugtenburg, Johan
Recueil des Travaux Chimiques des Pays-Bas, 1993 , vol. 112, # 1 p. 22 - 32
1: 43 percent / stannic chloride / 24 h / Ambient temperature
2: 95 percent / potassium hydroxide, hydrazine hydrate / various solvent(s) / 3 h / Heating
3: 63 percent / stannic chloride / 1,2-dichloro-ethane / 24 h
4: sodium dichromate / H2O / 18 h / 250 °C
5: 83 percent / acetic anhydride / Heating
View Scheme
参考文献
Hacker, Nigel P.; McOmie, John F. W.; Meunier-Piret, Jacqueline; Meerssche, Maurice Van
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 19 - 24
2-pyrazinyl-1-oxide in dichloromethane
Irradiationthe similar arene oxide formation (t.l.c. evidence) for acenaphthene;
参考文献
Akhtar, M. Naseem; Boyd, Derek R.; Neill, John D.; Jerina, Donald M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1693 - 1699