5-降冰片烯-2,3-二甲醇合成路线 （共 46 条）
参考文献
Calvet; Mejuto
Journal of the Chemical Society, 1936 , p. 554
反应条件
sulfuric acid
Einleiten von Chlorwasserstoff;
参考文献
Dharwarkar; Alimchandani
Journal of the Indian Chemical Society, 1940 , vol. 17, p. 416,419
参考文献
Science Union et Cie
Patent: US4338323 A1, 1982 ;
反应条件
1: urea; sodium isopropylate 2: palladium/charcoal; ethanol / Hydrogenation View Scheme
参考文献
Cope; Hancock
Journal of the American Chemical Society, 1939 , vol. 61, p. 776,779
反应条件
ethanol; sodium ethanolate
T=-10 - -5°C; und beim folgenden Kochen mit Aethyljodid;
参考文献
Cope; Hancock
Journal of the American Chemical Society, 1938 , vol. 60, p. 2904,2905
反应条件
sodium isopropanolate
T=60°C; dann bei 25grad, und Kochen mit Diaethylsulfat;
参考文献
Cope; Hancock
Journal of the American Chemical Society, 1938 , vol. 60, p. 2904,2905
反应条件
sodium hydroxide; water
T=40°C; Cannizzaro reaction; 0.5 h;
参考文献
Karpiak; Marshalok; Fedevich; Avdosieva; Kovalskyi, Ya. P.
Chemistry of Heterocyclic Compounds, 2008 , vol. 44, # 11 p. 1334 - 1338
反应条件
barium dihydroxide; water
参考文献
Chaudron; Pallaud
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1959 , vol. 249, p. 2212
Full Text Show Details
Pallaud et al.
Chimie et Industrie (Paris), 1963 , vol. 89, p. 283,289
反应条件
1: ZnCl2
2: H2 / Ni / ethanol / 150 °C / 110326 Torr
3: Na2Cr2O7, H2SO4
4: monoperoxyphthalic acid / diethyl ether
View Scheme
参考文献
Muehlstaedt,M.; Richter,P.
Chemische Berichte, 1967 , vol. 100, p. 1892 - 1897
反应条件
1: H2 / Ni / ethanol / 150 °C / 110326 Torr
2: Na2Cr2O7, H2SO4
3: monoperoxyphthalic acid / diethyl ether
View Scheme
参考文献
Muehlstaedt,M.; Richter,P.
Chemische Berichte, 1967 , vol. 100, p. 1892 - 1897
