Alpha-苯酰乙酰苯胺合成路线 （共 35 条）
反应条件
KNO2; 18-crown-6 ether in tetrahydrofuran
T=25°C; 15 h; under argon or oxygen; MechanismProduct distribution;
参考文献
Balogh-Hergovich, E.; Speier, G.
Tetrahedron Letters, 1982 , vol. 23, # 43 p. 4473 - 4476
反应条件
potassium hydroxide; silver(l) oxide in acetonitrile
T=25°C; 1.5 h; Microwave irradiation; optical yield given as percent dediastereoselective reaction;
参考文献
Zhang, Zhiguo; Fang, Shiliang; Liu, Qingfeng; Zhang, Guisheng
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 927 - 932
反应条件
1: dichloromethane / 20 °C
2: tert.-butylhydroperoxide; trifluorormethanesulfonic acid; palladium diacetate; acetic acid / N,N-dimethyl acetamide / 5 h / 90 °C
View Scheme
参考文献
Yuan, Yu; Chen, Duanteng; Wang, Xiaowei
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3373 - 3379
反应条件
manganese triacetate in acetic acid
T=100°C; 0.116667 h; Further byproducts given;
参考文献
Nishino; Kurosawa
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 6 p. 1682 - 1687
反应条件
sodium acetate
Heating;
参考文献
Peet, Norton P.; Sunder, Shyam; Barbuch, Robert J.; Whalon, Michael R.; Huber, Edward W.; Huffman, John C.
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1611 - 1618
反应条件
sodium iodide
4 h; Heating;
参考文献
Kamal, Ahmed; Ramana, A. Venkata; Reddy, K. Srinivasa; Ramana, K. Venkata; Hari Babu; Prasad, B. Rajendra
Tetrahedron Letters, 2004 , vol. 45, # 44 p. 8187 - 8190
反应条件
1: 17 percent / manganese(III) acetate dihydrate / acetic acid / 0.37 h / 100 °C
2: 99 percent / pyridine
View Scheme
参考文献
Nishino; Kurosawa
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 6 p. 1682 - 1687
反应条件
1: 6 percent / manganese(III) acetate dihydrate / acetic acid / 0.2 h / Heating
2: 99 percent / pyridine
View Scheme
参考文献
Nishino; Kurosawa
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 6 p. 1682 - 1687
反应条件
potassium hydroxide; palladium
Hydrogenation;
参考文献
Ruggli; Hegedues
Helvetica Chimica Acta, 1941 , vol. 24, p. 703,714
反应条件
1: Raney nickel; ethyl acetate / Hydrogenation
2: chloroform; bromine
3: sulfuric acid
4: palladium; methanol. KOH-solution / Hydrogenation
View Scheme
参考文献
Ruggli; Hegedues
Helvetica Chimica Acta, 1941 , vol. 24, p. 703,714
