5-(2-乙酰氧基乙酰基)苯-1,2,3-三基三乙酸酯合成路线 （共 10 条）
反应条件
hydrogenchloride; formic acid
参考文献
Roux; Freudenberg
Justus Liebigs Annalen der Chemie, 1958 , vol. 613, p. 56,60
反应条件
1: hydrogen chloride; ethanol / ethyl acetate / 25 h 2: 220 mg / sodium hydroxide / H2O / 2.25 h / 0 - 20 °C View Scheme
参考文献
Kraus, Michael; Biskup, Ellen; Richling, Elke; Schreier, Peter
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 13 p. 1151 - 1162
参考文献
Reichel; Burkhart
Justus Liebigs Annalen der Chemie, 1938 , vol. 536, p. 164,168
反应条件
sulfuric acid; potassium acetate; acetic acid
T=100°C; 3 h;
参考文献
Kraus, Michael; Biskup, Ellen; Richling, Elke; Schreier, Peter
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 13 p. 1151 - 1162
反应条件
1: 81 percent / CHCl3; diethyl ether / 0.5 h / -10 °C
2: 87 percent / hydrogen chloride / dioxane; diethyl ether / 0.5 h / 10 °C
3: 75 percent / acetic acid; potassium acetate; H2SO4 / 3 h / 100 °C
View Scheme
参考文献
Kraus, Michael; Biskup, Ellen; Richling, Elke; Schreier, Peter
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 13 p. 1151 - 1162
反应条件
1: 91 percent / thionyl chloride / 1 h / 85 °C
2: 81 percent / CHCl3; diethyl ether / 0.5 h / -10 °C
3: 87 percent / hydrogen chloride / dioxane; diethyl ether / 0.5 h / 10 °C
4: 75 percent / acetic acid; potassium acetate; H2SO4 / 3 h / 100 °C
View Scheme
参考文献
Kraus, Michael; Biskup, Ellen; Richling, Elke; Schreier, Peter
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 13 p. 1151 - 1162
反应条件
1: 79 percent / 3 h / 110 °C
2: 91 percent / thionyl chloride / 1 h / 85 °C
3: 81 percent / CHCl3; diethyl ether / 0.5 h / -10 °C
4: 87 percent / hydrogen chloride / dioxane; diethyl ether / 0.5 h / 10 °C
5: 75 percent / acetic acid; potassium acetate; H2SO4 / 3 h / 100 °C
View Scheme
参考文献
Kraus, Michael; Biskup, Ellen; Richling, Elke; Schreier, Peter
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 13 p. 1151 - 1162
反应条件
1: 87 percent / hydrogen chloride / dioxane; diethyl ether / 0.5 h / 10 °C
2: 75 percent / acetic acid; potassium acetate; H2SO4 / 3 h / 100 °C
View Scheme
参考文献
Kraus, Michael; Biskup, Ellen; Richling, Elke; Schreier, Peter
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 13 p. 1151 - 1162
参考文献
Reynolds; Robinson
Journal of the Chemical Society, 1934 , p. 1039,1040
参考文献
Hayashi
Acta Phytochimica, 1934 , vol. 8, p. 65,81
Full Text Show Details
Bradley; Robinson; Schwarzenbach
Journal of the Chemical Society, 1930 , p. 796,811
