in chloroform
byproducts: ammonium sulfide; introduction of dry NH3 into a soln. of S4N3Cl in CHCl3;discoloration; pptn.;; filtration, evapn. of filtrate;;
参考文献
Muthmann, W.; Seitter, E.
Ber., 1897 , vol. 30, p. 627 - 631
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Gmelin Handbook: S: MVol.B3, 155, page 1858 - 1860
in water
dissolving S4N3Cl in HClO4 (70 percent), removal (exhaustion) of HCl;; pptn. on addn. of pure acetic acid, cooling (ice) and addn. of ether/acetone mixture (2:1); filtration; attempt of washing (mixture of ether/acetone) causes vigorous detonation;;
参考文献
Meuwsen, A.; Jakob, O.
Z. Anorg. Chem., 1950 , vol. 263, p. 200 - 212
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Gmelin Handbook: S: MVol.B3, 156, page 1860 - 1863
Shah, A. R.; Padma, D. K.; Murthy, A. R. V.
Indian J. Chem., 1971 , vol. 9, p. 885
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Gmelin Handbook: S: SVol.4a/b, 1.1.4.6, page 23 - 23
Shah, A. R.; Padma, D. K.; Murthy, A. R. V.
Indian J. Chem., 1971 , vol. 9, p. 885
Full Text Show Details
Gmelin Handbook: S: SVol.4a/b, 1.1.4.6, page 23 - 23
