1-(叔丁氧基羰基)-2-吡咯烷酮合成路线 （共 30 条）
反应条件
1: Dibal-H / -78 °C 2: PTSA View Scheme
参考文献
Su, Bo; Chen, Fazhong; Wang, Lizhong; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2014 , vol. 62, # 6 p. 1233 - 1239
反应条件
C17H23BN2O T=25°C; P=760.051 Torr; 0.6 h; Inert atmosphere; chemoselective reaction;
参考文献
Oishi, Shunsuke; Saito, Susumu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 22 p. 5395 - 5399
反应条件
C17H23BN2O T=25°C; P=760.051 Torr; 0.8 h; Inert atmosphere; chemoselective reaction;
参考文献
Oishi, Shunsuke; Saito, Susumu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 22 p. 5395 - 5399
反应条件
silica gel in dichloromethane 0.0166667 h; Irradiation;
参考文献
Siro, Jorge G.; Martin, Justina; Garcia-Navio, Jose L.; Remuinan, Modesto J.; Vaquero, Juan J.
Synlett, 1998 , # 2 p. 147 - 148
反应条件
cyclohexene T=229.3°C; P=26.5 Torr; Kinetics; Further Variations:PressuresTemperatures;
参考文献
Brusco, Yannely; Dominguez, Rosa M.; Rotinov, Alexandra; Herize, Armando; Cordova, Mary; Chuchani, Gabriel
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 12 p. 796 - 800
反应条件
diisobutylaluminium hydride in tetrahydrofuran T=-78°C;
参考文献
Su, Bo; Chen, Fazhong; Wang, Lizhong; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2014 , vol. 62, # 6 p. 1233 - 1239
反应条件
1: 1.) LiHMDS, n-BuLi / 1.) THF, 2.) THF 2: DIBAL-H / tetrahydrofuran / -78 °C 3: quinolinium camphorsulfonate / toluene / 80 °C 4: 82 percent / Et3Al / toluene 5: 1.) NaH 6: 1.) n-Bu3SnH, AIBN, 2.) Mg / 1.) benzene, 80 deg C, 1 h, 2.) MeOH, 24 h, room t. View Scheme
参考文献
Cossy, Janine; Cases, Manuel; Gomez Pardo, Domingo
Tetrahedron Letters, 1998 , vol. 39, # 16 p. 2331 - 2332
反应条件
Cp*RuCl{(C6H5)2P-(CH2)2NH2-κ2-P,N}; potassium tert-butylate; hydrogen in tert-butyl alcohol T=80°C; P=22502.3 Torr; 36 h; Autoclave;
参考文献
Angewandte Chemie - International Edition, , vol. 48, # 7 p. 1324 - 1327
反应条件
Cp*RuCl{(C6H5)2P-(CH2)2NH2-κ2-P,N}; potassium tert-butylate; hydrogen T=80°C; P=22502.3 Torr; Autoclave;
参考文献
Angewandte Chemie - International Edition, , vol. 48, # 7 p. 1324 - 1327
反应条件
Cp*RuCl{(C6H5)2P-(CH2)2NH2-κ2-P,N}; potassium tert-butylate; hydrogen T=80°C; P=22502.3 Torr; Autoclave;
参考文献
Angewandte Chemie - International Edition, , vol. 48, # 7 p. 1324 - 1327
