4-(1-哌啶甲基)苯硼酸频哪醇酯合成路线 （共 5 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 0.75 h;
参考文献
WO2009/10488 A1, ;
Page/Page column 57-58 ;
WO 2009/010488 A1
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Ma, Winson M. J.; James, Tony D.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 18 p. 4850 - 4853
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; dichloromethane T=80°C; 12 h;
参考文献
Journal of Medicinal Chemistry, , vol. 56, # 10 p. 3820 - 3832
