3,4,5-三甲氧基苯甲醛合成路线 （共 427 条）
反应条件
sulfuric acid T=107°C; 1 h;
参考文献
Schwartz, Alan
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 2213 - 2214
反应条件
1: 3,5-dibromo-4-hydroxy-benzaldehyde; sodium methylate With copper(l) chloride in methanol; N,N-dimethyl-formamide T=120°C; 3 h; 2: dimethyl sulfate With sodium hydroxide pH=8.5 - 9.3; 3 h;
参考文献
Ji, Ya-Fei; Zong, Zhi-Min; Wei, Xian-Yong
Synthetic Communications, 2002 , vol. 32, # 18 p. 2809 - 2814
反应条件
potassium carbonate in N,N-dimethyl-formamide HeatingInert atmosphere;
参考文献
Deveau, Amy M.; Costa, Nancy E.; Joshi, Elizabeth M.; Macdonald, Timothy L.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 12 p. 3522 - 3525
反应条件
water; TiF4 T=60°C; 24 h; screw-capped vial;
参考文献
Jung, Misuk; Yoon, Jieun; Kim, Hak Sung; Ryu, Jae-Sang
Synthesis, 2010 , # 16 art. no. F04310SS, p. 2713 - 2720
反应条件
1: 18 g / CuCl2 / dimethylformamide / 1 h / 120 °C 2: 9 g / K2CO3 / acetone / 2 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 294 - 295
反应条件
[C12mim][FeCl4]; periodic acid T=30°C; 1.5 h;
参考文献
Hu, Yu Lin; Liu, Qi Fa; Lu, Ting Ting; Lu, Ming
Catalysis Communications, 2010 , vol. 11, # 10 p. 923 - 927
反应条件
copper T=250°C; 0.25 h;
参考文献
Tetrahedron, , vol. 38, # 16 p. 2569 - 2580
反应条件
1: With [iron(II)(H2O)6](perchlorate)2 in methanol 2: With dihydrogen peroxide in acetonitrile
参考文献
Mekmouche, Yasmina
Angewandte Chemie - International Edition, 2001 , vol. 40, # 5 p. 949 - 952
反应条件
tetrafluoroboric acid; [Fe(bipy)3]2+ in water; acetonitrile 0.0833333 h; Ambient temperature;
参考文献
Murase, Masayuki; Kotani, Eiichi; Tobinaga, Seisho
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 9 p. 3595 - 3598
反应条件
lithium aluminium tetrahydride; dipyridinium dichromate 1.) THF, 2.) CH2Cl2; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 63, # 16 p. 5662 - 5665
